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6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate
The title compound, C(13)H(7)ClN(4)O·C(2)H(6)O, was synthesized by the reaction of 4-chlorobenzaldehyde, malononitrile and 10% sodium hydroxide solution in an aqueous medium. In the crystal structure, the crystal packing is stabilized by intermolecular N—H⋯N, O—H⋯O and N—H⋯O hydrogen bonds....
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2008
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962196/ https://www.ncbi.nlm.nih.gov/pubmed/21203277 http://dx.doi.org/10.1107/S1600536808022551 |
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author | Jia, Runhong Tu, ShuJiang |
author_facet | Jia, Runhong Tu, ShuJiang |
author_sort | Jia, Runhong |
collection | PubMed |
description | The title compound, C(13)H(7)ClN(4)O·C(2)H(6)O, was synthesized by the reaction of 4-chlorobenzaldehyde, malononitrile and 10% sodium hydroxide solution in an aqueous medium. In the crystal structure, the crystal packing is stabilized by intermolecular N—H⋯N, O—H⋯O and N—H⋯O hydrogen bonds. |
format | Text |
id | pubmed-2962196 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2008 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29621962010-12-30 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate Jia, Runhong Tu, ShuJiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(7)ClN(4)O·C(2)H(6)O, was synthesized by the reaction of 4-chlorobenzaldehyde, malononitrile and 10% sodium hydroxide solution in an aqueous medium. In the crystal structure, the crystal packing is stabilized by intermolecular N—H⋯N, O—H⋯O and N—H⋯O hydrogen bonds. International Union of Crystallography 2008-07-23 /pmc/articles/PMC2962196/ /pubmed/21203277 http://dx.doi.org/10.1107/S1600536808022551 Text en © Jia and Tu 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Jia, Runhong Tu, ShuJiang 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
title | 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
title_full | 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
title_fullStr | 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
title_full_unstemmed | 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
title_short | 6-Amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
title_sort | 6-amino-4-(4-chlorophenyl)-2-oxo-1,2-dihydropyridine-3,5-dicarbonitrile ethanol solvate |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962196/ https://www.ncbi.nlm.nih.gov/pubmed/21203277 http://dx.doi.org/10.1107/S1600536808022551 |
work_keys_str_mv | AT jiarunhong 6amino44chlorophenyl2oxo12dihydropyridine35dicarbonitrileethanolsolvate AT tushujiang 6amino44chlorophenyl2oxo12dihydropyridine35dicarbonitrileethanolsolvate |