r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one

In the title compound, C(21)H(25)NO(3), the piperidinone ring adopts a chair conformation with an equatorial orientation of all substituents; the 3-methoxy­phenyl groups make a dihedral angle of 60.26 (15)°. The carbonyl group O atom is disordered over two positions in a 0.643 (3):0.357 (3) ratio. T...

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Detalles Bibliográficos
Autores principales: Parthiban, P., Ramkumar, V., Kumar, Nanjundan Ashok, Kim, Jong Su, Jeong, Yeon Tae
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962197/
https://www.ncbi.nlm.nih.gov/pubmed/21203321
http://dx.doi.org/10.1107/S1600536808023490
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author Parthiban, P.
Ramkumar, V.
Kumar, Nanjundan Ashok
Kim, Jong Su
Jeong, Yeon Tae
author_facet Parthiban, P.
Ramkumar, V.
Kumar, Nanjundan Ashok
Kim, Jong Su
Jeong, Yeon Tae
author_sort Parthiban, P.
collection PubMed
description In the title compound, C(21)H(25)NO(3), the piperidinone ring adopts a chair conformation with an equatorial orientation of all substituents; the 3-methoxy­phenyl groups make a dihedral angle of 60.26 (15)°. The carbonyl group O atom is disordered over two positions in a 0.643 (3):0.357 (3) ratio. The crystal structure is stabilized by N—H⋯O and C—H⋯O hydrogen bonding.
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spelling pubmed-29621972010-12-30 r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one Parthiban, P. Ramkumar, V. Kumar, Nanjundan Ashok Kim, Jong Su Jeong, Yeon Tae Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(21)H(25)NO(3), the piperidinone ring adopts a chair conformation with an equatorial orientation of all substituents; the 3-methoxy­phenyl groups make a dihedral angle of 60.26 (15)°. The carbonyl group O atom is disordered over two positions in a 0.643 (3):0.357 (3) ratio. The crystal structure is stabilized by N—H⋯O and C—H⋯O hydrogen bonding. International Union of Crystallography 2008-07-31 /pmc/articles/PMC2962197/ /pubmed/21203321 http://dx.doi.org/10.1107/S1600536808023490 Text en © Parthiban et al. 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Parthiban, P.
Ramkumar, V.
Kumar, Nanjundan Ashok
Kim, Jong Su
Jeong, Yeon Tae
r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
title r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
title_full r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
title_fullStr r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
title_full_unstemmed r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
title_short r-2,c-6-Bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
title_sort r-2,c-6-bis(3-methoxy­phen­yl)-t-3,t-5-dimethyl­piperidin-4-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962197/
https://www.ncbi.nlm.nih.gov/pubmed/21203321
http://dx.doi.org/10.1107/S1600536808023490
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