N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate

The title compound, C(17)H(17)BrN(2)O(4)·CH(4)O, was synthesized by the condensation of 3,4,5-trimethoxy­benzohydrazide and 2-bromo­benzaldehyde. The two aromatic rings are approximately planar, the dihedral angle being 3.08 (9)°. The mol­ecules are linked by inter­molecular N—H⋯O and O—H⋯O hydrogen...

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Detalles Bibliográficos
Autores principales: Zhu, Yong-Chuang, He, Dao-Hang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962239/
https://www.ncbi.nlm.nih.gov/pubmed/21203320
http://dx.doi.org/10.1107/S1600536808021764
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author Zhu, Yong-Chuang
He, Dao-Hang
author_facet Zhu, Yong-Chuang
He, Dao-Hang
author_sort Zhu, Yong-Chuang
collection PubMed
description The title compound, C(17)H(17)BrN(2)O(4)·CH(4)O, was synthesized by the condensation of 3,4,5-trimethoxy­benzohydrazide and 2-bromo­benzaldehyde. The two aromatic rings are approximately planar, the dihedral angle being 3.08 (9)°. The mol­ecules are linked by inter­molecular N—H⋯O and O—H⋯O hydrogen bonds into chains along the a axis.
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spelling pubmed-29622392010-12-30 N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate Zhu, Yong-Chuang He, Dao-Hang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(17)BrN(2)O(4)·CH(4)O, was synthesized by the condensation of 3,4,5-trimethoxy­benzohydrazide and 2-bromo­benzaldehyde. The two aromatic rings are approximately planar, the dihedral angle being 3.08 (9)°. The mol­ecules are linked by inter­molecular N—H⋯O and O—H⋯O hydrogen bonds into chains along the a axis. International Union of Crystallography 2008-07-31 /pmc/articles/PMC2962239/ /pubmed/21203320 http://dx.doi.org/10.1107/S1600536808021764 Text en © Zhu and He 2008 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhu, Yong-Chuang
He, Dao-Hang
N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
title N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
title_full N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
title_fullStr N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
title_full_unstemmed N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
title_short N′-(2-Bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
title_sort n′-(2-bromo­benzyl­idene)-3,4,5-tri­methoxy­benzohydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962239/
https://www.ncbi.nlm.nih.gov/pubmed/21203320
http://dx.doi.org/10.1107/S1600536808021764
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AT hedaohang n2bromobenzylidene345trimethoxybenzohydrazidemethanolsolvate

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