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Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method
In this study, silver nanoparticles (Ag-NPs) were synthesized using the wet chemical reduction method on the external surface layer of talc mineral as a solid support. Silver nitrate and sodium borohydride were used as the silver precursor and reducing agent in talc. The talc was suspended in aqueou...
Autores principales: | , , , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
Dove Medical Press
2010
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962270/ https://www.ncbi.nlm.nih.gov/pubmed/21042420 http://dx.doi.org/10.2147/IJN.S13227 |
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author | Shameli, Kamyar Ahmad, Mansor Bin Yunus, Wan Zin Wan Ibrahim, Nor Azowa Darroudi, Majid |
author_facet | Shameli, Kamyar Ahmad, Mansor Bin Yunus, Wan Zin Wan Ibrahim, Nor Azowa Darroudi, Majid |
author_sort | Shameli, Kamyar |
collection | PubMed |
description | In this study, silver nanoparticles (Ag-NPs) were synthesized using the wet chemical reduction method on the external surface layer of talc mineral as a solid support. Silver nitrate and sodium borohydride were used as the silver precursor and reducing agent in talc. The talc was suspended in aqueous AgNO(3) solution. After the absorption of Ag(+) on the surface, the ions were reduced with NaBH(4). The interlamellar space limits were without many changes (d(s) = 9.34–9.19 A(º)); therefore, Ag-NPs formed on the exterior surface of talc, with d(ave) = 7.60–13.11 nm in diameter. The properties of Ag/talc nanocomposites (Ag/talc-NCs) and the diameters of the Ag-NPs prepared in this way depended on the primary AgNO(3) concentration. The prepared Ag-NPs were characterized by ultraviolet-visible spectroscopy, powder X-ray diffraction, transmission electron microscopy, scanning electron microscopy, and Fourier transform infrared. These Ag/talc-NCs may have potential applications in the chemical and biological industries. |
format | Text |
id | pubmed-2962270 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2010 |
publisher | Dove Medical Press |
record_format | MEDLINE/PubMed |
spelling | pubmed-29622702010-11-01 Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method Shameli, Kamyar Ahmad, Mansor Bin Yunus, Wan Zin Wan Ibrahim, Nor Azowa Darroudi, Majid Int J Nanomedicine Original Research In this study, silver nanoparticles (Ag-NPs) were synthesized using the wet chemical reduction method on the external surface layer of talc mineral as a solid support. Silver nitrate and sodium borohydride were used as the silver precursor and reducing agent in talc. The talc was suspended in aqueous AgNO(3) solution. After the absorption of Ag(+) on the surface, the ions were reduced with NaBH(4). The interlamellar space limits were without many changes (d(s) = 9.34–9.19 A(º)); therefore, Ag-NPs formed on the exterior surface of talc, with d(ave) = 7.60–13.11 nm in diameter. The properties of Ag/talc nanocomposites (Ag/talc-NCs) and the diameters of the Ag-NPs prepared in this way depended on the primary AgNO(3) concentration. The prepared Ag-NPs were characterized by ultraviolet-visible spectroscopy, powder X-ray diffraction, transmission electron microscopy, scanning electron microscopy, and Fourier transform infrared. These Ag/talc-NCs may have potential applications in the chemical and biological industries. Dove Medical Press 2010-10-05 2010 /pmc/articles/PMC2962270/ /pubmed/21042420 http://dx.doi.org/10.2147/IJN.S13227 Text en © 2010 Shameli et al, publisher and licensee Dove Medical Press Ltd. This is an Open Access article which permits unrestricted noncommercial use, provided the original work is properly cited. |
spellingShingle | Original Research Shameli, Kamyar Ahmad, Mansor Bin Yunus, Wan Zin Wan Ibrahim, Nor Azowa Darroudi, Majid Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
title | Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
title_full | Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
title_fullStr | Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
title_full_unstemmed | Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
title_short | Synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
title_sort | synthesis and characterization of silver/talc nanocomposites using the wet chemical reduction method |
topic | Original Research |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2962270/ https://www.ncbi.nlm.nih.gov/pubmed/21042420 http://dx.doi.org/10.2147/IJN.S13227 |
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