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N′-(2-Hydr­oxy-3-methoxy­benzyl­idene)-1,3-benzodioxole-5-carbohydrazide monohydrate

Single crystals of the title compound, C(16)H(14)N(2)O(5)·H(2)O, were obtained from a condensation reaction of 1,3-benzodioxole-5-carbohydrazide and 3-methoxy­salicylaldehyde in a 95% ethanol solution. The asymmetric unit consists of a Schiff base mol­ecule, which assumes an E configuration with res...

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Detalles Bibliográficos
Autor principal: Du, Chun-Lin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2967948/
https://www.ncbi.nlm.nih.gov/pubmed/21581672
http://dx.doi.org/10.1107/S1600536808040117
Descripción
Sumario:Single crystals of the title compound, C(16)H(14)N(2)O(5)·H(2)O, were obtained from a condensation reaction of 1,3-benzodioxole-5-carbohydrazide and 3-methoxy­salicylaldehyde in a 95% ethanol solution. The asymmetric unit consists of a Schiff base mol­ecule, which assumes an E configuration with respect to the C=N bond, and a water mol­ecule of crystallization. The dihedral angle between the two substituted benzene rings is 12.7 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds, forming layers parallel to the bc plane.