2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one

In the centrosymmetric title compound, C(34)H(30)F(2)N(6)O(4), the dihedral angle between the quinazolinone and fluorobenzene ring planes are 71.00 (2) and 74.94 (2)° and an intra­molecular N—H⋯O interaction stabilizes the conformation. In the crystal, C—H⋯F and C—H⋯O links help to establish the pac...

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Detalles Bibliográficos
Autores principales: Wang, Xiang, Ma, Zuan, Chen, Yu-Lu
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2967967/
https://www.ncbi.nlm.nih.gov/pubmed/21581694
http://dx.doi.org/10.1107/S1600536808040841
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author Wang, Xiang
Ma, Zuan
Chen, Yu-Lu
author_facet Wang, Xiang
Ma, Zuan
Chen, Yu-Lu
author_sort Wang, Xiang
collection PubMed
description In the centrosymmetric title compound, C(34)H(30)F(2)N(6)O(4), the dihedral angle between the quinazolinone and fluorobenzene ring planes are 71.00 (2) and 74.94 (2)° and an intra­molecular N—H⋯O interaction stabilizes the conformation. In the crystal, C—H⋯F and C—H⋯O links help to establish the packing.
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spelling pubmed-29679672010-12-30 2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one Wang, Xiang Ma, Zuan Chen, Yu-Lu Acta Crystallogr Sect E Struct Rep Online Organic Papers In the centrosymmetric title compound, C(34)H(30)F(2)N(6)O(4), the dihedral angle between the quinazolinone and fluorobenzene ring planes are 71.00 (2) and 74.94 (2)° and an intra­molecular N—H⋯O interaction stabilizes the conformation. In the crystal, C—H⋯F and C—H⋯O links help to establish the packing. International Union of Crystallography 2008-12-10 /pmc/articles/PMC2967967/ /pubmed/21581694 http://dx.doi.org/10.1107/S1600536808040841 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Xiang
Ma, Zuan
Chen, Yu-Lu
2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one
title 2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one
title_full 2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one
title_fullStr 2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one
title_full_unstemmed 2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one
title_short 2,2′-Bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3H)-one
title_sort 2,2′-bis(4-fluoro­anilino)-3,3′-(3,6-dioxa­octane-1,8-di­yl)diquinazolin-4(3h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2967967/
https://www.ncbi.nlm.nih.gov/pubmed/21581694
http://dx.doi.org/10.1107/S1600536808040841
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