3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide

The title compound, C(19)H(12)F(2)N(2)O(2), a 2:1 product of the reaction of 3-fluoro­benzoyl­chloride and 2-amino­pyridine crystallizes with a disordered 3-fluoro­benzene ring adopting two conformations [ratio of occupancies 0.959 (4):0.041 (4)]. In the crystal structure, there are no classical hyd...

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Detalles Bibliográficos
Autores principales: Gallagher, John F., Donnelly, Katie, Lough, Alan J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968027/
https://www.ncbi.nlm.nih.gov/pubmed/21581566
http://dx.doi.org/10.1107/S1600536808041093
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author Gallagher, John F.
Donnelly, Katie
Lough, Alan J.
author_facet Gallagher, John F.
Donnelly, Katie
Lough, Alan J.
author_sort Gallagher, John F.
collection PubMed
description The title compound, C(19)H(12)F(2)N(2)O(2), a 2:1 product of the reaction of 3-fluoro­benzoyl­chloride and 2-amino­pyridine crystallizes with a disordered 3-fluoro­benzene ring adopting two conformations [ratio of occupancies 0.959 (4):0.041 (4)]. In the crystal structure, there are no classical hydrogen bonds and inter­actions comprise C—H⋯O in the form 2(C—H)⋯O=C [with motif R (2) (1)(5)]; C—H⋯π(arene) inter­actions are also present.
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spelling pubmed-29680272010-12-30 3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide Gallagher, John F. Donnelly, Katie Lough, Alan J. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(12)F(2)N(2)O(2), a 2:1 product of the reaction of 3-fluoro­benzoyl­chloride and 2-amino­pyridine crystallizes with a disordered 3-fluoro­benzene ring adopting two conformations [ratio of occupancies 0.959 (4):0.041 (4)]. In the crystal structure, there are no classical hydrogen bonds and inter­actions comprise C—H⋯O in the form 2(C—H)⋯O=C [with motif R (2) (1)(5)]; C—H⋯π(arene) inter­actions are also present. International Union of Crystallography 2008-12-13 /pmc/articles/PMC2968027/ /pubmed/21581566 http://dx.doi.org/10.1107/S1600536808041093 Text en © Gallagher et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Gallagher, John F.
Donnelly, Katie
Lough, Alan J.
3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide
title 3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide
title_full 3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide
title_fullStr 3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide
title_full_unstemmed 3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide
title_short 3-Fluoro-N-(3-fluoro­benzo­yl)-N-(2-pyrid­yl)benzamide
title_sort 3-fluoro-n-(3-fluoro­benzo­yl)-n-(2-pyrid­yl)benzamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968027/
https://www.ncbi.nlm.nih.gov/pubmed/21581566
http://dx.doi.org/10.1107/S1600536808041093
work_keys_str_mv AT gallagherjohnf 3fluoron3fluorobenzoyln2pyridylbenzamide
AT donnellykatie 3fluoron3fluorobenzoyln2pyridylbenzamide
AT loughalanj 3fluoron3fluorobenzoyln2pyridylbenzamide

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