N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide

The mol­ecule of the title compound, C(16)H(24)N(2)O(6), which lies on a crystallographic inversion centre in the centre of the benzene ring, adopts an anti conformation in terms of the relative orientation of two amide carbonyl groups. One pair of the 2-hydroxy­ethyl groups is partially disordered...

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Autores principales: Wang, Zhi-Qiang, Xu, Chen, Li, Ying-Fei, Cen, Fei-Fei, Zhang, Yu-Qing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2008
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968077/
https://www.ncbi.nlm.nih.gov/pubmed/21581622
http://dx.doi.org/10.1107/S1600536808041573
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author Wang, Zhi-Qiang
Xu, Chen
Li, Ying-Fei
Cen, Fei-Fei
Zhang, Yu-Qing
author_facet Wang, Zhi-Qiang
Xu, Chen
Li, Ying-Fei
Cen, Fei-Fei
Zhang, Yu-Qing
author_sort Wang, Zhi-Qiang
collection PubMed
description The mol­ecule of the title compound, C(16)H(24)N(2)O(6), which lies on a crystallographic inversion centre in the centre of the benzene ring, adopts an anti conformation in terms of the relative orientation of two amide carbonyl groups. One pair of the 2-hydroxy­ethyl groups is partially disordered with site occupancy factors of 0.811 (2) and 0.189 (2). The dihedral angle between the amide group and central benzene ring is 67.0 (2)°. Two O—H⋯O and one bifurcated O—H⋯(O,O) hydrogen bonds are present, resulting in a three-dimensional network.
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spelling pubmed-29680772010-12-30 N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide Wang, Zhi-Qiang Xu, Chen Li, Ying-Fei Cen, Fei-Fei Zhang, Yu-Qing Acta Crystallogr Sect E Struct Rep Online Organic Papers The mol­ecule of the title compound, C(16)H(24)N(2)O(6), which lies on a crystallographic inversion centre in the centre of the benzene ring, adopts an anti conformation in terms of the relative orientation of two amide carbonyl groups. One pair of the 2-hydroxy­ethyl groups is partially disordered with site occupancy factors of 0.811 (2) and 0.189 (2). The dihedral angle between the amide group and central benzene ring is 67.0 (2)°. Two O—H⋯O and one bifurcated O—H⋯(O,O) hydrogen bonds are present, resulting in a three-dimensional network. International Union of Crystallography 2008-12-20 /pmc/articles/PMC2968077/ /pubmed/21581622 http://dx.doi.org/10.1107/S1600536808041573 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Zhi-Qiang
Xu, Chen
Li, Ying-Fei
Cen, Fei-Fei
Zhang, Yu-Qing
N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide
title N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide
title_full N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide
title_fullStr N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide
title_full_unstemmed N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide
title_short N,N,N′,N′-Tetra­kis(2-hydroxy­ethyl)terephthalamide
title_sort n,n,n′,n′-tetra­kis(2-hydroxy­ethyl)terephthalamide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968077/
https://www.ncbi.nlm.nih.gov/pubmed/21581622
http://dx.doi.org/10.1107/S1600536808041573
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