4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate

The title compound, crystallized as a methanol solvate, C(18)H(20)O(2)·CH(3)OH, is an inter­mediate in the synthesis of the anti­lipidemic agent clinofibrate. Mol­ecules are packed together with the methanol solvent molecule via two O—H⋯O hydrogen bonds. The third O—H⋯O hydrogen bond is between neig...

Descripción completa

Detalles Bibliográficos
Autores principales: Shuai, Jun, Liu, Ying, Liu, Mo, Liu, Dengke
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968192/
https://www.ncbi.nlm.nih.gov/pubmed/21581883
http://dx.doi.org/10.1107/S1600536809000427
_version_ 1782189800927789056
author Shuai, Jun
Liu, Ying
Liu, Mo
Liu, Dengke
author_facet Shuai, Jun
Liu, Ying
Liu, Mo
Liu, Dengke
author_sort Shuai, Jun
collection PubMed
description The title compound, crystallized as a methanol solvate, C(18)H(20)O(2)·CH(3)OH, is an inter­mediate in the synthesis of the anti­lipidemic agent clinofibrate. Mol­ecules are packed together with the methanol solvent molecule via two O—H⋯O hydrogen bonds. The third O—H⋯O hydrogen bond is between neighboring 4,4′-(cyclo­hexane-1,1-di­yl)diphenol mol­ecules. The dihedral angle between two benzene rings planes is 81.69 (6).
format Text
id pubmed-2968192
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29681922010-12-30 4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate Shuai, Jun Liu, Ying Liu, Mo Liu, Dengke Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, crystallized as a methanol solvate, C(18)H(20)O(2)·CH(3)OH, is an inter­mediate in the synthesis of the anti­lipidemic agent clinofibrate. Mol­ecules are packed together with the methanol solvent molecule via two O—H⋯O hydrogen bonds. The third O—H⋯O hydrogen bond is between neighboring 4,4′-(cyclo­hexane-1,1-di­yl)diphenol mol­ecules. The dihedral angle between two benzene rings planes is 81.69 (6). International Union of Crystallography 2009-01-10 /pmc/articles/PMC2968192/ /pubmed/21581883 http://dx.doi.org/10.1107/S1600536809000427 Text en © Shuai et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Shuai, Jun
Liu, Ying
Liu, Mo
Liu, Dengke
4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate
title 4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate
title_full 4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate
title_fullStr 4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate
title_full_unstemmed 4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate
title_short 4,4′-(Cyclo­hexane-1,1-di­yl)diphenol methanol solvate
title_sort 4,4′-(cyclo­hexane-1,1-di­yl)diphenol methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968192/
https://www.ncbi.nlm.nih.gov/pubmed/21581883
http://dx.doi.org/10.1107/S1600536809000427
work_keys_str_mv AT shuaijun 44cyclohexane11diyldiphenolmethanolsolvate
AT liuying 44cyclohexane11diyldiphenolmethanolsolvate
AT liumo 44cyclohexane11diyldiphenolmethanolsolvate
AT liudengke 44cyclohexane11diyldiphenolmethanolsolvate

Ejemplares similares