Pyridine-2-carbaldehyde thio­semi­carbazone

The asymmetric unit of the title compound, C(7)H(8)N(4)S, contains two independent mol­ecules with slightly different conformations; the dihedral angles between the pyridine ring and mean plane of the thio­semicarbazone unit in the two mol­ecules are 2.88 (5) and 6.30 (5)°. Inter­molecular N—H⋯N and...

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Detalles Bibliográficos
Autores principales: Song, Li-Hua, Zhang, Xiang, Jiang, Kun, Yang, Sheng-Xiang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968221/
https://www.ncbi.nlm.nih.gov/pubmed/21581955
http://dx.doi.org/10.1107/S1600536809001962
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author Song, Li-Hua
Zhang, Xiang
Jiang, Kun
Yang, Sheng-Xiang
author_facet Song, Li-Hua
Zhang, Xiang
Jiang, Kun
Yang, Sheng-Xiang
author_sort Song, Li-Hua
collection PubMed
description The asymmetric unit of the title compound, C(7)H(8)N(4)S, contains two independent mol­ecules with slightly different conformations; the dihedral angles between the pyridine ring and mean plane of the thio­semicarbazone unit in the two mol­ecules are 2.88 (5) and 6.30 (5)°. Inter­molecular N—H⋯N and N—H⋯S hydrogen bonds link the mol­ecules into layers parallel to the ab plane.
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spelling pubmed-29682212010-12-30 Pyridine-2-carbaldehyde thio­semi­carbazone Song, Li-Hua Zhang, Xiang Jiang, Kun Yang, Sheng-Xiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(7)H(8)N(4)S, contains two independent mol­ecules with slightly different conformations; the dihedral angles between the pyridine ring and mean plane of the thio­semicarbazone unit in the two mol­ecules are 2.88 (5) and 6.30 (5)°. Inter­molecular N—H⋯N and N—H⋯S hydrogen bonds link the mol­ecules into layers parallel to the ab plane. International Union of Crystallography 2009-01-23 /pmc/articles/PMC2968221/ /pubmed/21581955 http://dx.doi.org/10.1107/S1600536809001962 Text en © Song et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Song, Li-Hua
Zhang, Xiang
Jiang, Kun
Yang, Sheng-Xiang
Pyridine-2-carbaldehyde thio­semi­carbazone
title Pyridine-2-carbaldehyde thio­semi­carbazone
title_full Pyridine-2-carbaldehyde thio­semi­carbazone
title_fullStr Pyridine-2-carbaldehyde thio­semi­carbazone
title_full_unstemmed Pyridine-2-carbaldehyde thio­semi­carbazone
title_short Pyridine-2-carbaldehyde thio­semi­carbazone
title_sort pyridine-2-carbaldehyde thio­semi­carbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968221/
https://www.ncbi.nlm.nih.gov/pubmed/21581955
http://dx.doi.org/10.1107/S1600536809001962
work_keys_str_mv AT songlihua pyridine2carbaldehydethiosemicarbazone
AT zhangxiang pyridine2carbaldehydethiosemicarbazone
AT jiangkun pyridine2carbaldehydethiosemicarbazone
AT yangshengxiang pyridine2carbaldehydethiosemicarbazone

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