1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate

In the title compound, C(16)H(24)N(4)O(9)S(2)·H(2)O, the hexopyranosyl ring adopts a chair conformation ((4) C (1)), and the five substituents are in equatorial positions. In the crystal structure, extensive O—H⋯O, N—H⋯S and N—H⋯O hydrogen bonding leads to the formation of a three-dimensional networ...

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Detalles Bibliográficos
Autores principales: Sun, Weidong, Yao, Jin, Bai, Lifei, Wang, Xiaoming
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968307/
https://www.ncbi.nlm.nih.gov/pubmed/21581859
http://dx.doi.org/10.1107/S1600536808043833
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author Sun, Weidong
Yao, Jin
Bai, Lifei
Wang, Xiaoming
author_facet Sun, Weidong
Yao, Jin
Bai, Lifei
Wang, Xiaoming
author_sort Sun, Weidong
collection PubMed
description In the title compound, C(16)H(24)N(4)O(9)S(2)·H(2)O, the hexopyranosyl ring adopts a chair conformation ((4) C (1)), and the five substituents are in equatorial positions. In the crystal structure, extensive O—H⋯O, N—H⋯S and N—H⋯O hydrogen bonding leads to the formation of a three-dimensional network.
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spelling pubmed-29683072010-12-30 1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate Sun, Weidong Yao, Jin Bai, Lifei Wang, Xiaoming Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(16)H(24)N(4)O(9)S(2)·H(2)O, the hexopyranosyl ring adopts a chair conformation ((4) C (1)), and the five substituents are in equatorial positions. In the crystal structure, extensive O—H⋯O, N—H⋯S and N—H⋯O hydrogen bonding leads to the formation of a three-dimensional network. International Union of Crystallography 2009-01-08 /pmc/articles/PMC2968307/ /pubmed/21581859 http://dx.doi.org/10.1107/S1600536808043833 Text en © Sun et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Sun, Weidong
Yao, Jin
Bai, Lifei
Wang, Xiaoming
1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
title 1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
title_full 1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
title_fullStr 1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
title_full_unstemmed 1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
title_short 1-(2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
title_sort 1-(2,3,4,6-tetra-o-acetyl-β-d-gluco­pyranos­yl)-3-thio­ureidothio­urea monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968307/
https://www.ncbi.nlm.nih.gov/pubmed/21581859
http://dx.doi.org/10.1107/S1600536808043833
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