Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate

The asymmetric unit of the title compound, C(16)H(10)O(8)·2H(2)O, contains one-half of the centrosymmetric organic mol­ecule and one water mol­ecule. The dihedral angles between the carboxyl­ate groups and the adjacent phenyl ring are 71.31 (3) and 16.67 (3)°, while the carboxyl­ate groups are orien...

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Detalles Bibliográficos
Autores principales: Li, Fei, Wang, Wu-Wei, Ji, Xing, Cao, Chang-Chun, Zhu, Dong-Ya
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968332/
https://www.ncbi.nlm.nih.gov/pubmed/21581861
http://dx.doi.org/10.1107/S1600536808044012
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author Li, Fei
Wang, Wu-Wei
Ji, Xing
Cao, Chang-Chun
Zhu, Dong-Ya
author_facet Li, Fei
Wang, Wu-Wei
Ji, Xing
Cao, Chang-Chun
Zhu, Dong-Ya
author_sort Li, Fei
collection PubMed
description The asymmetric unit of the title compound, C(16)H(10)O(8)·2H(2)O, contains one-half of the centrosymmetric organic mol­ecule and one water mol­ecule. The dihedral angles between the carboxyl­ate groups and the adjacent phenyl ring are 71.31 (3) and 16.67 (3)°, while the carboxyl­ate groups are oriented at a dihedral angle of 72.01 (3)°. In the crystal structure, inter­molecular O—H⋯O and bifurcated O—H⋯(O,O) hydrogen bonds link the mol­ecules to form a three-dimensional supra­molecular network.
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spelling pubmed-29683322010-12-30 Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate Li, Fei Wang, Wu-Wei Ji, Xing Cao, Chang-Chun Zhu, Dong-Ya Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(16)H(10)O(8)·2H(2)O, contains one-half of the centrosymmetric organic mol­ecule and one water mol­ecule. The dihedral angles between the carboxyl­ate groups and the adjacent phenyl ring are 71.31 (3) and 16.67 (3)°, while the carboxyl­ate groups are oriented at a dihedral angle of 72.01 (3)°. In the crystal structure, inter­molecular O—H⋯O and bifurcated O—H⋯(O,O) hydrogen bonds link the mol­ecules to form a three-dimensional supra­molecular network. International Union of Crystallography 2009-01-08 /pmc/articles/PMC2968332/ /pubmed/21581861 http://dx.doi.org/10.1107/S1600536808044012 Text en © Li et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Fei
Wang, Wu-Wei
Ji, Xing
Cao, Chang-Chun
Zhu, Dong-Ya
Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
title Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
title_full Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
title_fullStr Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
title_full_unstemmed Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
title_short Biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
title_sort biphenyl-3,3′,4,4′-tetra­carboxylic acid dihydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968332/
https://www.ncbi.nlm.nih.gov/pubmed/21581861
http://dx.doi.org/10.1107/S1600536808044012
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AT wangwuwei biphenyl3344tetracarboxylicaciddihydrate
AT jixing biphenyl3344tetracarboxylicaciddihydrate
AT caochangchun biphenyl3344tetracarboxylicaciddihydrate
AT zhudongya biphenyl3344tetracarboxylicaciddihydrate

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