1-Benzoyl-3-(5-quinol­yl)thio­urea

The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio­cyanate and 5-amino­quinoline in the presence of polyethyl­eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol­ecules linked by N—H⋯N and C—H⋯N hydrogen b...

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Detalles Bibliográficos
Autores principales: Du, Wen-Hu, Wei, Chang-Mei, Wang, Wei-Feng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968342/
https://www.ncbi.nlm.nih.gov/pubmed/21581917
http://dx.doi.org/10.1107/S1600536809000932
Descripción
Sumario:The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio­cyanate and 5-amino­quinoline in the presence of polyethyl­eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol­ecules linked by N—H⋯N and C—H⋯N hydrogen bonds involving all the potential donors, generating sheets parallel to (100). An intramolecular N—H⋯O bond is also present.

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