1-Benzoyl-3-(5-quinol­yl)thio­urea

The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio­cyanate and 5-amino­quinoline in the presence of polyethyl­eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol­ecules linked by N—H⋯N and C—H⋯N hydrogen b...

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Detalles Bibliográficos
Autores principales: Du, Wen-Hu, Wei, Chang-Mei, Wang, Wei-Feng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968342/
https://www.ncbi.nlm.nih.gov/pubmed/21581917
http://dx.doi.org/10.1107/S1600536809000932
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author Du, Wen-Hu
Wei, Chang-Mei
Wang, Wei-Feng
author_facet Du, Wen-Hu
Wei, Chang-Mei
Wang, Wei-Feng
author_sort Du, Wen-Hu
collection PubMed
description The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio­cyanate and 5-amino­quinoline in the presence of polyethyl­eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol­ecules linked by N—H⋯N and C—H⋯N hydrogen bonds involving all the potential donors, generating sheets parallel to (100). An intramolecular N—H⋯O bond is also present.
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spelling pubmed-29683422010-12-30 1-Benzoyl-3-(5-quinol­yl)thio­urea Du, Wen-Hu Wei, Chang-Mei Wang, Wei-Feng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(13)N(3)OS, was obtained by the reaction of benzoyl chloride, ammonium thio­cyanate and 5-amino­quinoline in the presence of polyethyl­eneglycol-400 (PEG-400) as a phase-transfer catalyst. The compound crystallized as discrete mol­ecules linked by N—H⋯N and C—H⋯N hydrogen bonds involving all the potential donors, generating sheets parallel to (100). An intramolecular N—H⋯O bond is also present. International Union of Crystallography 2009-01-14 /pmc/articles/PMC2968342/ /pubmed/21581917 http://dx.doi.org/10.1107/S1600536809000932 Text en © Du et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Du, Wen-Hu
Wei, Chang-Mei
Wang, Wei-Feng
1-Benzoyl-3-(5-quinol­yl)thio­urea
title 1-Benzoyl-3-(5-quinol­yl)thio­urea
title_full 1-Benzoyl-3-(5-quinol­yl)thio­urea
title_fullStr 1-Benzoyl-3-(5-quinol­yl)thio­urea
title_full_unstemmed 1-Benzoyl-3-(5-quinol­yl)thio­urea
title_short 1-Benzoyl-3-(5-quinol­yl)thio­urea
title_sort 1-benzoyl-3-(5-quinol­yl)thio­urea
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968342/
https://www.ncbi.nlm.nih.gov/pubmed/21581917
http://dx.doi.org/10.1107/S1600536809000932
work_keys_str_mv AT duwenhu 1benzoyl35quinolylthiourea
AT weichangmei 1benzoyl35quinolylthiourea
AT wangweifeng 1benzoyl35quinolylthiourea

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