4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione

The title compound, C(9)H(11)N(3)S(2), exists in the thione form in the crystal structure. The central triazole ring is almost perpendicular to the thio­phene ring which is disordered over two orientations [dihedral angles of 88.5 (7) and 85.7 (8)° for the two orientations]. The crystal structure is...

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Detalles Bibliográficos
Autores principales: Wujec, Monika, Mazur, Liliana, Rzączyńska, Zofia
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968376/
https://www.ncbi.nlm.nih.gov/pubmed/21581888
http://dx.doi.org/10.1107/S1600536809000440
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author Wujec, Monika
Mazur, Liliana
Rzączyńska, Zofia
author_facet Wujec, Monika
Mazur, Liliana
Rzączyńska, Zofia
author_sort Wujec, Monika
collection PubMed
description The title compound, C(9)H(11)N(3)S(2), exists in the thione form in the crystal structure. The central triazole ring is almost perpendicular to the thio­phene ring which is disordered over two orientations [dihedral angles of 88.5 (7) and 85.7 (8)° for the two orientations]. The crystal structure is stabilized by strong inter­molecular N—H⋯S hydrogen bonds, forming centrosymmetric dimers, and by some weak C—H⋯S inter­actions.
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spelling pubmed-29683762010-12-30 4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione Wujec, Monika Mazur, Liliana Rzączyńska, Zofia Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(9)H(11)N(3)S(2), exists in the thione form in the crystal structure. The central triazole ring is almost perpendicular to the thio­phene ring which is disordered over two orientations [dihedral angles of 88.5 (7) and 85.7 (8)° for the two orientations]. The crystal structure is stabilized by strong inter­molecular N—H⋯S hydrogen bonds, forming centrosymmetric dimers, and by some weak C—H⋯S inter­actions. International Union of Crystallography 2009-01-10 /pmc/articles/PMC2968376/ /pubmed/21581888 http://dx.doi.org/10.1107/S1600536809000440 Text en © Wujec et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wujec, Monika
Mazur, Liliana
Rzączyńska, Zofia
4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione
title 4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione
title_full 4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione
title_fullStr 4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione
title_full_unstemmed 4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione
title_short 4-Ethyl-3-(2-thienylmeth­yl)-Δ(2)-1,2,4-triazoline-5-thione
title_sort 4-ethyl-3-(2-thienylmeth­yl)-δ(2)-1,2,4-triazoline-5-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968376/
https://www.ncbi.nlm.nih.gov/pubmed/21581888
http://dx.doi.org/10.1107/S1600536809000440
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AT mazurliliana 4ethyl32thienylmethyld2124triazoline5thione
AT rzaczynskazofia 4ethyl32thienylmethyld2124triazoline5thione

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