N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate

In the title compound, C(15)H(13)N(3)O(4)·CH(3)OH, the dihedral angle between the two substituted benzene rings is 66.7 (2)°. An intra­molecular O—H⋯N hydrogen bond is observed in the Schiff base mol­ecule. In the crystal structure, the Schiff base and solvent mol­ecules are linked into chains runni...

Descripción completa

Detalles Bibliográficos
Autores principales: Xiao, Ge-Jiang, Wei, Chao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968426/
https://www.ncbi.nlm.nih.gov/pubmed/21582240
http://dx.doi.org/10.1107/S160053680900508X
_version_ 1782189872779362304
author Xiao, Ge-Jiang
Wei, Chao
author_facet Xiao, Ge-Jiang
Wei, Chao
author_sort Xiao, Ge-Jiang
collection PubMed
description In the title compound, C(15)H(13)N(3)O(4)·CH(3)OH, the dihedral angle between the two substituted benzene rings is 66.7 (2)°. An intra­molecular O—H⋯N hydrogen bond is observed in the Schiff base mol­ecule. In the crystal structure, the Schiff base and solvent mol­ecules are linked into chains running along the a axis by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds.
format Text
id pubmed-2968426
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29684262010-12-30 N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate Xiao, Ge-Jiang Wei, Chao Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(15)H(13)N(3)O(4)·CH(3)OH, the dihedral angle between the two substituted benzene rings is 66.7 (2)°. An intra­molecular O—H⋯N hydrogen bond is observed in the Schiff base mol­ecule. In the crystal structure, the Schiff base and solvent mol­ecules are linked into chains running along the a axis by inter­molecular O—H⋯O and N—H⋯O hydrogen bonds. International Union of Crystallography 2009-02-25 /pmc/articles/PMC2968426/ /pubmed/21582240 http://dx.doi.org/10.1107/S160053680900508X Text en © Xiao and Wei 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Xiao, Ge-Jiang
Wei, Chao
N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
title N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
title_full N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
title_fullStr N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
title_full_unstemmed N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
title_short N′-[1-(2-Hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
title_sort n′-[1-(2-hydroxy­phen­yl)ethyl­idene]-2-nitro­benzohydrazide methanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968426/
https://www.ncbi.nlm.nih.gov/pubmed/21582240
http://dx.doi.org/10.1107/S160053680900508X
work_keys_str_mv AT xiaogejiang n12hydroxyphenylethylidene2nitrobenzohydrazidemethanolsolvate
AT weichao n12hydroxyphenylethylidene2nitrobenzohydrazidemethanolsolvate

Ejemplares similares