N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide

The title compound, C(13)H(9)ClN(4)O(3), was synthesized by the condensation reaction of 2-chloro-5-nitro­benzaldehyde with isonicotinohydrazide in a methanol solution. The mol­ecule of the compound displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the...

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Detalles Bibliográficos
Autor principal: Zhi, Feng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968476/
https://www.ncbi.nlm.nih.gov/pubmed/21582275
http://dx.doi.org/10.1107/S1600536809006588
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author Zhi, Feng
author_facet Zhi, Feng
author_sort Zhi, Feng
collection PubMed
description The title compound, C(13)H(9)ClN(4)O(3), was synthesized by the condensation reaction of 2-chloro-5-nitro­benzaldehyde with isonicotinohydrazide in a methanol solution. The mol­ecule of the compound displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the benzene and pyridine rings is 12.1 (2)°. In the crystal structure, adjacent mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds, forming dimers.
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spelling pubmed-29684762010-12-30 N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide Zhi, Feng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(9)ClN(4)O(3), was synthesized by the condensation reaction of 2-chloro-5-nitro­benzaldehyde with isonicotinohydrazide in a methanol solution. The mol­ecule of the compound displays a trans configuration with respect to the C=N and C—N bonds. The dihedral angle between the benzene and pyridine rings is 12.1 (2)°. In the crystal structure, adjacent mol­ecules are linked through inter­molecular N—H⋯O hydrogen bonds, forming dimers. International Union of Crystallography 2009-02-28 /pmc/articles/PMC2968476/ /pubmed/21582275 http://dx.doi.org/10.1107/S1600536809006588 Text en © Feng Zhi 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhi, Feng
N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide
title N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide
title_full N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide
title_fullStr N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide
title_full_unstemmed N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide
title_short N′-(2-Chloro-5-nitro­benzyl­idene)isonicotinohydrazide
title_sort n′-(2-chloro-5-nitro­benzyl­idene)isonicotinohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968476/
https://www.ncbi.nlm.nih.gov/pubmed/21582275
http://dx.doi.org/10.1107/S1600536809006588
work_keys_str_mv AT zhifeng n2chloro5nitrobenzylideneisonicotinohydrazide

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