3-Methoxy­benzaldehyde thio­semi­carbazone

The title compound, C(9)H(11)N(3)OS, was prepared by the reaction of 3-methoxy­benzaldehyde and thio­semicarbazide. The benzyl­idene ring and the thio­semicarbazone fragment are slightly twisted, making a dihedral angle of 14.1 (1)°. A weak intra­molecular N—H⋯N hydrogen bond may influence the confo...

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Detalles Bibliográficos
Autores principales: Zhang, Jian, Wu, Lin-ping, Zhuang, Ling-hua, Wang, Guo-wei
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968893/
https://www.ncbi.nlm.nih.gov/pubmed/21582593
http://dx.doi.org/10.1107/S160053680901040X
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author Zhang, Jian
Wu, Lin-ping
Zhuang, Ling-hua
Wang, Guo-wei
author_facet Zhang, Jian
Wu, Lin-ping
Zhuang, Ling-hua
Wang, Guo-wei
author_sort Zhang, Jian
collection PubMed
description The title compound, C(9)H(11)N(3)OS, was prepared by the reaction of 3-methoxy­benzaldehyde and thio­semicarbazide. The benzyl­idene ring and the thio­semicarbazone fragment are slightly twisted, making a dihedral angle of 14.1 (1)°. A weak intra­molecular N—H⋯N hydrogen bond may influence the conformation of the mol­ecule. Inter­molecular N—H⋯S hydrogen bonds build up a three-dimensional network.
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spelling pubmed-29688932010-12-30 3-Methoxy­benzaldehyde thio­semi­carbazone Zhang, Jian Wu, Lin-ping Zhuang, Ling-hua Wang, Guo-wei Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(9)H(11)N(3)OS, was prepared by the reaction of 3-methoxy­benzaldehyde and thio­semicarbazide. The benzyl­idene ring and the thio­semicarbazone fragment are slightly twisted, making a dihedral angle of 14.1 (1)°. A weak intra­molecular N—H⋯N hydrogen bond may influence the conformation of the mol­ecule. Inter­molecular N—H⋯S hydrogen bonds build up a three-dimensional network. International Union of Crystallography 2009-03-28 /pmc/articles/PMC2968893/ /pubmed/21582593 http://dx.doi.org/10.1107/S160053680901040X Text en © Zhang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Zhang, Jian
Wu, Lin-ping
Zhuang, Ling-hua
Wang, Guo-wei
3-Methoxy­benzaldehyde thio­semi­carbazone
title 3-Methoxy­benzaldehyde thio­semi­carbazone
title_full 3-Methoxy­benzaldehyde thio­semi­carbazone
title_fullStr 3-Methoxy­benzaldehyde thio­semi­carbazone
title_full_unstemmed 3-Methoxy­benzaldehyde thio­semi­carbazone
title_short 3-Methoxy­benzaldehyde thio­semi­carbazone
title_sort 3-methoxy­benzaldehyde thio­semi­carbazone
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968893/
https://www.ncbi.nlm.nih.gov/pubmed/21582593
http://dx.doi.org/10.1107/S160053680901040X
work_keys_str_mv AT zhangjian 3methoxybenzaldehydethiosemicarbazone
AT wulinping 3methoxybenzaldehydethiosemicarbazone
AT zhuanglinghua 3methoxybenzaldehydethiosemicarbazone
AT wangguowei 3methoxybenzaldehydethiosemicarbazone

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