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(E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one

The title compound, C(17)H(16)ClNO, was synthesized using a solvent-free method by reaction of 4-(dimethyl­amino)benzaldehyde with 4-chloro­acetophenone and NaOH. The chloro­phenyl ring makes a dihedral angle of 18.1 (3)° with the central propenone unit, while the (dimethyl­amino)phenyl group is dis...

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Detalles Bibliográficos
Autores principales: Lei, Xinyou, Bai, Xiaohua
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968919/
https://www.ncbi.nlm.nih.gov/pubmed/21582472
http://dx.doi.org/10.1107/S1600536809007430
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author Lei, Xinyou
Bai, Xiaohua
author_facet Lei, Xinyou
Bai, Xiaohua
author_sort Lei, Xinyou
collection PubMed
description The title compound, C(17)H(16)ClNO, was synthesized using a solvent-free method by reaction of 4-(dimethyl­amino)benzaldehyde with 4-chloro­acetophenone and NaOH. The chloro­phenyl ring makes a dihedral angle of 18.1 (3)° with the central propenone unit, while the (dimethyl­amino)phenyl group is disordered over two orientations of equal occupancies, which make dihedral angles with the central propenone unit of 32.9 (3) and 57.4 (3)°, respectively.
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spelling pubmed-29689192010-12-30 (E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one Lei, Xinyou Bai, Xiaohua Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(16)ClNO, was synthesized using a solvent-free method by reaction of 4-(dimethyl­amino)benzaldehyde with 4-chloro­acetophenone and NaOH. The chloro­phenyl ring makes a dihedral angle of 18.1 (3)° with the central propenone unit, while the (dimethyl­amino)phenyl group is disordered over two orientations of equal occupancies, which make dihedral angles with the central propenone unit of 32.9 (3) and 57.4 (3)°, respectively. International Union of Crystallography 2009-03-11 /pmc/articles/PMC2968919/ /pubmed/21582472 http://dx.doi.org/10.1107/S1600536809007430 Text en © Lei and Bai 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Lei, Xinyou
Bai, Xiaohua
(E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
title (E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
title_full (E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
title_fullStr (E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
title_full_unstemmed (E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
title_short (E)-1-(4-Chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
title_sort (e)-1-(4-chloro­phen­yl)-3-[4-(dimethyl­amino)phen­yl]prop-2-en-1-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968919/
https://www.ncbi.nlm.nih.gov/pubmed/21582472
http://dx.doi.org/10.1107/S1600536809007430
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