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(E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one
The title compound, C(17)H(16)ClNO, was synthesized using a solvent-free method by reaction of 4-(dimethylamino)benzaldehyde with 4-chloroacetophenone and NaOH. The chlorophenyl ring makes a dihedral angle of 18.1 (3)° with the central propenone unit, while the (dimethylamino)phenyl group is dis...
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Formato: | Texto |
Lenguaje: | English |
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International Union of Crystallography
2009
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Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968919/ https://www.ncbi.nlm.nih.gov/pubmed/21582472 http://dx.doi.org/10.1107/S1600536809007430 |
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author | Lei, Xinyou Bai, Xiaohua |
author_facet | Lei, Xinyou Bai, Xiaohua |
author_sort | Lei, Xinyou |
collection | PubMed |
description | The title compound, C(17)H(16)ClNO, was synthesized using a solvent-free method by reaction of 4-(dimethylamino)benzaldehyde with 4-chloroacetophenone and NaOH. The chlorophenyl ring makes a dihedral angle of 18.1 (3)° with the central propenone unit, while the (dimethylamino)phenyl group is disordered over two orientations of equal occupancies, which make dihedral angles with the central propenone unit of 32.9 (3) and 57.4 (3)°, respectively. |
format | Text |
id | pubmed-2968919 |
institution | National Center for Biotechnology Information |
language | English |
publishDate | 2009 |
publisher | International Union of Crystallography |
record_format | MEDLINE/PubMed |
spelling | pubmed-29689192010-12-30 (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one Lei, Xinyou Bai, Xiaohua Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(17)H(16)ClNO, was synthesized using a solvent-free method by reaction of 4-(dimethylamino)benzaldehyde with 4-chloroacetophenone and NaOH. The chlorophenyl ring makes a dihedral angle of 18.1 (3)° with the central propenone unit, while the (dimethylamino)phenyl group is disordered over two orientations of equal occupancies, which make dihedral angles with the central propenone unit of 32.9 (3) and 57.4 (3)°, respectively. International Union of Crystallography 2009-03-11 /pmc/articles/PMC2968919/ /pubmed/21582472 http://dx.doi.org/10.1107/S1600536809007430 Text en © Lei and Bai 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
spellingShingle | Organic Papers Lei, Xinyou Bai, Xiaohua (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
title | (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
title_full | (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
title_fullStr | (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
title_full_unstemmed | (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
title_short | (E)-1-(4-Chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
title_sort | (e)-1-(4-chlorophenyl)-3-[4-(dimethylamino)phenyl]prop-2-en-1-one |
topic | Organic Papers |
url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968919/ https://www.ncbi.nlm.nih.gov/pubmed/21582472 http://dx.doi.org/10.1107/S1600536809007430 |
work_keys_str_mv | AT leixinyou e14chlorophenyl34dimethylaminophenylprop2en1one AT baixiaohua e14chlorophenyl34dimethylaminophenylprop2en1one |