(E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate

In the title compound, C(14)H(11)ClN(2)O(4)·H(2)O, the dihedral angle between the two benzene rings is 8.5 (2)° and an intra­molecular O—H⋯N hydrogen bond is observed in the Schiff base mol­ecule. In the crystal structure, the water mol­ecule accepts an N—H⋯O hydrogen bond and makes O—H⋯O hydrogen b...

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Detalles Bibliográficos
Autores principales: Deng, Sa, Han, Ling, Huang, Shan-shan, Zhang, Hou-li, Diao, Yun-peng, Liu, Ke-xin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968927/
https://www.ncbi.nlm.nih.gov/pubmed/21582457
http://dx.doi.org/10.1107/S1600536809007788
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author Deng, Sa
Han, Ling
Huang, Shan-shan
Zhang, Hou-li
Diao, Yun-peng
Liu, Ke-xin
author_facet Deng, Sa
Han, Ling
Huang, Shan-shan
Zhang, Hou-li
Diao, Yun-peng
Liu, Ke-xin
author_sort Deng, Sa
collection PubMed
description In the title compound, C(14)H(11)ClN(2)O(4)·H(2)O, the dihedral angle between the two benzene rings is 8.5 (2)° and an intra­molecular O—H⋯N hydrogen bond is observed in the Schiff base mol­ecule. In the crystal structure, the water mol­ecule accepts an N—H⋯O hydrogen bond and makes O—H⋯O hydrogen bonds to two further Schiff base mol­ecules. Further inter­molecular O—H⋯O hydrogen bonds lead to the formation of layers parallel to the bc plane.
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spelling pubmed-29689272010-12-30 (E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate Deng, Sa Han, Ling Huang, Shan-shan Zhang, Hou-li Diao, Yun-peng Liu, Ke-xin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(11)ClN(2)O(4)·H(2)O, the dihedral angle between the two benzene rings is 8.5 (2)° and an intra­molecular O—H⋯N hydrogen bond is observed in the Schiff base mol­ecule. In the crystal structure, the water mol­ecule accepts an N—H⋯O hydrogen bond and makes O—H⋯O hydrogen bonds to two further Schiff base mol­ecules. Further inter­molecular O—H⋯O hydrogen bonds lead to the formation of layers parallel to the bc plane. International Union of Crystallography 2009-03-11 /pmc/articles/PMC2968927/ /pubmed/21582457 http://dx.doi.org/10.1107/S1600536809007788 Text en © Deng et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Deng, Sa
Han, Ling
Huang, Shan-shan
Zhang, Hou-li
Diao, Yun-peng
Liu, Ke-xin
(E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
title (E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
title_full (E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
title_fullStr (E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
title_full_unstemmed (E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
title_short (E)-N′-(5-Chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
title_sort (e)-n′-(5-chloro-2-hydroxy­benzyl­idene)-3,5-dihydroxy­benzohydrazide mono­hydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2968927/
https://www.ncbi.nlm.nih.gov/pubmed/21582457
http://dx.doi.org/10.1107/S1600536809007788
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