2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate

In the main mol­ecule of the title compound, C(22)H(20)N(2)O(4)·1.13CH(4)O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent mol­ecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13)...

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Autores principales: Al-Douh, Mohammed H., Osman, Hasnah, Hamid, Shafida A., Kia, Reza, Fun, Hoong-Kun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969071/
https://www.ncbi.nlm.nih.gov/pubmed/21582627
http://dx.doi.org/10.1107/S1600536809011192
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author Al-Douh, Mohammed H.
Osman, Hasnah
Hamid, Shafida A.
Kia, Reza
Fun, Hoong-Kun
author_facet Al-Douh, Mohammed H.
Osman, Hasnah
Hamid, Shafida A.
Kia, Reza
Fun, Hoong-Kun
author_sort Al-Douh, Mohammed H.
collection PubMed
description In the main mol­ecule of the title compound, C(22)H(20)N(2)O(4)·1.13CH(4)O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent mol­ecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (5). The crystal structure is stabilized by inter­molecular O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917 (1)/0.083 (1)].
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spelling pubmed-29690712010-12-30 2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate Al-Douh, Mohammed H. Osman, Hasnah Hamid, Shafida A. Kia, Reza Fun, Hoong-Kun Acta Crystallogr Sect E Struct Rep Online Organic Papers In the main mol­ecule of the title compound, C(22)H(20)N(2)O(4)·1.13CH(4)O, the dihedral angles between the benzimidazole plane and the two benzene rings are 80.53 (10) and 82.76 (10)°. The solvent mol­ecules are disordered between three positions, with refined occupancies of 0.506 (13), 0.373 (13) and 0.249 (5). The crystal structure is stabilized by inter­molecular O—H⋯O, O—H⋯N and C—H⋯O hydrogen bonds. The crystal studied was a merohedral twin [BASF ratio of 0.917 (1)/0.083 (1)]. International Union of Crystallography 2009-03-31 /pmc/articles/PMC2969071/ /pubmed/21582627 http://dx.doi.org/10.1107/S1600536809011192 Text en © Al-Douh et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Al-Douh, Mohammed H.
Osman, Hasnah
Hamid, Shafida A.
Kia, Reza
Fun, Hoong-Kun
2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
title 2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
title_full 2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
title_fullStr 2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
title_full_unstemmed 2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
title_short 2-[1-(2-Hydr­oxy-3-methoxy­benz­yl)-1H-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
title_sort 2-[1-(2-hydr­oxy-3-methoxy­benz­yl)-1h-benzimidazol-2-yl]-6-methoxy­phenol methanol 1.13-solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969071/
https://www.ncbi.nlm.nih.gov/pubmed/21582627
http://dx.doi.org/10.1107/S1600536809011192
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