tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate

The reaction of (E)-tert-butyl 4-[3-(dimethyl­amino)acrylo­yl]piperidine-1-carboxyl­ate with methyl­hydrazine leads to the formation of the title compound, C(14)H(23)N(3)O(2), with a 1-methyl-1H-pyrazol-5-yl substituent. The plane of the pyrazole ring forms a dihedral angle of 33.4 (1)° with the app...

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Detalles Bibliográficos
Autores principales: Richter, Daniel, Kath, John C., Rheingold, Arnold L., DiPasquale, Antonio, Yanovsky, Alex
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969088/
https://www.ncbi.nlm.nih.gov/pubmed/21582582
http://dx.doi.org/10.1107/S1600536809010332
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author Richter, Daniel
Kath, John C.
Rheingold, Arnold L.
DiPasquale, Antonio
Yanovsky, Alex
author_facet Richter, Daniel
Kath, John C.
Rheingold, Arnold L.
DiPasquale, Antonio
Yanovsky, Alex
author_sort Richter, Daniel
collection PubMed
description The reaction of (E)-tert-butyl 4-[3-(dimethyl­amino)acrylo­yl]piperidine-1-carboxyl­ate with methyl­hydrazine leads to the formation of the title compound, C(14)H(23)N(3)O(2), with a 1-methyl-1H-pyrazol-5-yl substituent. The plane of the pyrazole ring forms a dihedral angle of 33.4 (1)° with the approximate mirror plane of the piperidine ring.
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spelling pubmed-29690882010-12-30 tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate Richter, Daniel Kath, John C. Rheingold, Arnold L. DiPasquale, Antonio Yanovsky, Alex Acta Crystallogr Sect E Struct Rep Online Organic Papers The reaction of (E)-tert-butyl 4-[3-(dimethyl­amino)acrylo­yl]piperidine-1-carboxyl­ate with methyl­hydrazine leads to the formation of the title compound, C(14)H(23)N(3)O(2), with a 1-methyl-1H-pyrazol-5-yl substituent. The plane of the pyrazole ring forms a dihedral angle of 33.4 (1)° with the approximate mirror plane of the piperidine ring. International Union of Crystallography 2009-03-25 /pmc/articles/PMC2969088/ /pubmed/21582582 http://dx.doi.org/10.1107/S1600536809010332 Text en © Richter et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Richter, Daniel
Kath, John C.
Rheingold, Arnold L.
DiPasquale, Antonio
Yanovsky, Alex
tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate
title tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate
title_full tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate
title_fullStr tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate
title_full_unstemmed tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate
title_short tert-Butyl 4-(1-methyl-1H-pyrazol-5-yl)piperidine-1-carboxyl­ate
title_sort tert-butyl 4-(1-methyl-1h-pyrazol-5-yl)piperidine-1-carboxyl­ate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969088/
https://www.ncbi.nlm.nih.gov/pubmed/21582582
http://dx.doi.org/10.1107/S1600536809010332
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AT dipasqualeantonio tertbutyl41methyl1hpyrazol5ylpiperidine1carboxylate
AT yanovskyalex tertbutyl41methyl1hpyrazol5ylpiperidine1carboxylate

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