2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione

In the title mol­ecule, C(24)H(26)Cl(2)N(6)S(2), the two phenyl rings form a dihedral angle of 51.95 (7)° and the distance between their centroids is 4.156 (8) Å. The crystal packing exhibits weak inter­molecular C—H⋯S and C—H⋯N hydrogen bonds.

Detalles Bibliográficos
Autores principales: Wu, Yandong, Sun, Yichong
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969207/
https://www.ncbi.nlm.nih.gov/pubmed/21582966
http://dx.doi.org/10.1107/S1600536809024118
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author Wu, Yandong
Sun, Yichong
author_facet Wu, Yandong
Sun, Yichong
author_sort Wu, Yandong
collection PubMed
description In the title mol­ecule, C(24)H(26)Cl(2)N(6)S(2), the two phenyl rings form a dihedral angle of 51.95 (7)° and the distance between their centroids is 4.156 (8) Å. The crystal packing exhibits weak inter­molecular C—H⋯S and C—H⋯N hydrogen bonds.
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spelling pubmed-29692072010-12-30 2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione Wu, Yandong Sun, Yichong Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(24)H(26)Cl(2)N(6)S(2), the two phenyl rings form a dihedral angle of 51.95 (7)° and the distance between their centroids is 4.156 (8) Å. The crystal packing exhibits weak inter­molecular C—H⋯S and C—H⋯N hydrogen bonds. International Union of Crystallography 2009-06-27 /pmc/articles/PMC2969207/ /pubmed/21582966 http://dx.doi.org/10.1107/S1600536809024118 Text en © Wu and Sun 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wu, Yandong
Sun, Yichong
2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title 2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_full 2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_fullStr 2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_full_unstemmed 2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_short 2,6-Bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_sort 2,6-bis(2-chloro­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969207/
https://www.ncbi.nlm.nih.gov/pubmed/21582966
http://dx.doi.org/10.1107/S1600536809024118
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AT sunyichong 26bis2chloroethyl8b8cdiphenylperhydro23a4a67a8ahexaazacyclopentadeffluorene48dithione

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