rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)

The title compound, C(8)H(10)O(5)·C(2)H(3)N(3)S·H(2)O, was synthesized by the reaction of 2-amino-1,3,4-thia­diazole with norcantharidin. The crystal structure is stabilized by N—H⋯O, N—H⋯N, O—H⋯O and O—H⋯N hydrogen bonds. In addition, weak π–π inter­actions are observed between symmetry-related thi...

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Detalles Bibliográficos
Autores principales: Wang, Na, Lin, Qiu-Yue, Wang, Yan-Jun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969213/
https://www.ncbi.nlm.nih.gov/pubmed/21582865
http://dx.doi.org/10.1107/S1600536809021825
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author Wang, Na
Lin, Qiu-Yue
Wang, Yan-Jun
author_facet Wang, Na
Lin, Qiu-Yue
Wang, Yan-Jun
author_sort Wang, Na
collection PubMed
description The title compound, C(8)H(10)O(5)·C(2)H(3)N(3)S·H(2)O, was synthesized by the reaction of 2-amino-1,3,4-thia­diazole with norcantharidin. The crystal structure is stabilized by N—H⋯O, N—H⋯N, O—H⋯O and O—H⋯N hydrogen bonds. In addition, weak π–π inter­actions are observed between symmetry-related thia­diazole ring systems [centroid–centroid distance = 3.9110 (3) Å, inter­planar spacing = 3.4845 Å].
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spelling pubmed-29692132010-12-30 rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1) Wang, Na Lin, Qiu-Yue Wang, Yan-Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(8)H(10)O(5)·C(2)H(3)N(3)S·H(2)O, was synthesized by the reaction of 2-amino-1,3,4-thia­diazole with norcantharidin. The crystal structure is stabilized by N—H⋯O, N—H⋯N, O—H⋯O and O—H⋯N hydrogen bonds. In addition, weak π–π inter­actions are observed between symmetry-related thia­diazole ring systems [centroid–centroid distance = 3.9110 (3) Å, inter­planar spacing = 3.4845 Å]. International Union of Crystallography 2009-06-17 /pmc/articles/PMC2969213/ /pubmed/21582865 http://dx.doi.org/10.1107/S1600536809021825 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Na
Lin, Qiu-Yue
Wang, Yan-Jun
rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
title rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
title_full rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
title_fullStr rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
title_full_unstemmed rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
title_short rac-7-Oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
title_sort rac-7-oxabicyclo­[2.2.1]heptane-2,3-dicarboxylic acid–2-amino-1,3,4-thia­diazole–water (1/1/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969213/
https://www.ncbi.nlm.nih.gov/pubmed/21582865
http://dx.doi.org/10.1107/S1600536809021825
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AT linqiuyue rac7oxabicyclo221heptane23dicarboxylicacid2amino134thiadiazolewater111
AT wangyanjun rac7oxabicyclo221heptane23dicarboxylicacid2amino134thiadiazolewater111

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