4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione

In the title mol­ecule, C(9)H(12)S(5)O, the five-membered ring and attached S atom are essentially coplanar [mean deviation from the mean plane = 0.020 (1) Å]. The two S atoms belonging to the macrocycle deviate from this plane by 1.005 (1) and 1.337 (2) Å. In the crystal, π–π inter­actions link the...

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Detalles Bibliográficos
Autores principales: Hou, Rui-Bin, Li, Bao, Yin, Bing-Zhu, Wu, Li-Xin
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969415/
https://www.ncbi.nlm.nih.gov/pubmed/21582961
http://dx.doi.org/10.1107/S1600536809024003
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author Hou, Rui-Bin
Li, Bao
Yin, Bing-Zhu
Wu, Li-Xin
author_facet Hou, Rui-Bin
Li, Bao
Yin, Bing-Zhu
Wu, Li-Xin
author_sort Hou, Rui-Bin
collection PubMed
description In the title mol­ecule, C(9)H(12)S(5)O, the five-membered ring and attached S atom are essentially coplanar [mean deviation from the mean plane = 0.020 (1) Å]. The two S atoms belonging to the macrocycle deviate from this plane by 1.005 (1) and 1.337 (2) Å. In the crystal, π–π inter­actions link the mol­ecules into centrosymmetric dimers with a short distance of 3.753 (5) Å between the centroids of the five-membered rings.
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spelling pubmed-29694152010-12-30 4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione Hou, Rui-Bin Li, Bao Yin, Bing-Zhu Wu, Li-Xin Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(9)H(12)S(5)O, the five-membered ring and attached S atom are essentially coplanar [mean deviation from the mean plane = 0.020 (1) Å]. The two S atoms belonging to the macrocycle deviate from this plane by 1.005 (1) and 1.337 (2) Å. In the crystal, π–π inter­actions link the mol­ecules into centrosymmetric dimers with a short distance of 3.753 (5) Å between the centroids of the five-membered rings. International Union of Crystallography 2009-06-27 /pmc/articles/PMC2969415/ /pubmed/21582961 http://dx.doi.org/10.1107/S1600536809024003 Text en © Hou et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Hou, Rui-Bin
Li, Bao
Yin, Bing-Zhu
Wu, Li-Xin
4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
title 4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
title_full 4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
title_fullStr 4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
title_full_unstemmed 4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
title_short 4,6,7,9,10,12-Hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
title_sort 4,6,7,9,10,12-hexahydro-1,3-dithiolo[4,5-f][1,4,9]oxadithia­cyclo­undecine-2-thione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969415/
https://www.ncbi.nlm.nih.gov/pubmed/21582961
http://dx.doi.org/10.1107/S1600536809024003
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