5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine

The title compound, C(13)H(17)N(3)S, was synthesized by the reaction of 4-pentyl­benzoic acid and thio­semicarbazide. The dihedral angle between the thia­diazole and phenyl rings is 29.9 (2)°. An intra­molecular C—H⋯S inter­action is observed. In the crystal, inter­molecular N—H⋯N hydrogen bonding l...

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Detalles Bibliográficos
Autores principales: Wang, Yao, Wan, Rong, Han, Feng, Wang, Peng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969462/
https://www.ncbi.nlm.nih.gov/pubmed/21582881
http://dx.doi.org/10.1107/S1600536809022594
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author Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
author_facet Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
author_sort Wang, Yao
collection PubMed
description The title compound, C(13)H(17)N(3)S, was synthesized by the reaction of 4-pentyl­benzoic acid and thio­semicarbazide. The dihedral angle between the thia­diazole and phenyl rings is 29.9 (2)°. An intra­molecular C—H⋯S inter­action is observed. In the crystal, inter­molecular N—H⋯N hydrogen bonding links the mol­ecules into centrosymmetric dimers.
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spelling pubmed-29694622010-12-30 5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine Wang, Yao Wan, Rong Han, Feng Wang, Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(13)H(17)N(3)S, was synthesized by the reaction of 4-pentyl­benzoic acid and thio­semicarbazide. The dihedral angle between the thia­diazole and phenyl rings is 29.9 (2)°. An intra­molecular C—H⋯S inter­action is observed. In the crystal, inter­molecular N—H⋯N hydrogen bonding links the mol­ecules into centrosymmetric dimers. International Union of Crystallography 2009-06-17 /pmc/articles/PMC2969462/ /pubmed/21582881 http://dx.doi.org/10.1107/S1600536809022594 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
title 5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
title_full 5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
title_fullStr 5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
title_full_unstemmed 5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
title_short 5-(4-Pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
title_sort 5-(4-pentyl­phen­yl)-1,3,4-thia­diazol-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969462/
https://www.ncbi.nlm.nih.gov/pubmed/21582881
http://dx.doi.org/10.1107/S1600536809022594
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AT wanrong 54pentylphenyl134thiadiazol2amine
AT hanfeng 54pentylphenyl134thiadiazol2amine
AT wangpeng 54pentylphenyl134thiadiazol2amine

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