Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K

There are two independent mol­ecules in the asymmetric unit of the title compound, C(13)H(23)NO(5)S. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into two independent one-dimensional chains along [100]. The crystal studied was found to be a non-merohedral twin with...

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Autores principales: Singh, Suneel P., Verdu, Marcus J., Lough, Alan J., Schwan, Adrian L.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969554/
https://www.ncbi.nlm.nih.gov/pubmed/21583234
http://dx.doi.org/10.1107/S1600536809019011
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author Singh, Suneel P.
Verdu, Marcus J.
Lough, Alan J.
Schwan, Adrian L.
author_facet Singh, Suneel P.
Verdu, Marcus J.
Lough, Alan J.
Schwan, Adrian L.
author_sort Singh, Suneel P.
collection PubMed
description There are two independent mol­ecules in the asymmetric unit of the title compound, C(13)H(23)NO(5)S. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into two independent one-dimensional chains along [100]. The crystal studied was found to be a non-merohedral twin with a ratio of 0.615 (6):0.385 (1) for the refined components. At 200 (1) K [Singh et al. (2009 ▶). Acta Cryst. E65, o1385–o1386] the crystal structure of the title compound contains one disordered mol­ecule in the asymmetric unit of a monoclinic unit cell.
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spelling pubmed-29695542010-12-30 Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K Singh, Suneel P. Verdu, Marcus J. Lough, Alan J. Schwan, Adrian L. Acta Crystallogr Sect E Struct Rep Online Organic Papers There are two independent mol­ecules in the asymmetric unit of the title compound, C(13)H(23)NO(5)S. In the crystal structure, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into two independent one-dimensional chains along [100]. The crystal studied was found to be a non-merohedral twin with a ratio of 0.615 (6):0.385 (1) for the refined components. At 200 (1) K [Singh et al. (2009 ▶). Acta Cryst. E65, o1385–o1386] the crystal structure of the title compound contains one disordered mol­ecule in the asymmetric unit of a monoclinic unit cell. International Union of Crystallography 2009-05-23 /pmc/articles/PMC2969554/ /pubmed/21583234 http://dx.doi.org/10.1107/S1600536809019011 Text en © Singh et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Singh, Suneel P.
Verdu, Marcus J.
Lough, Alan J.
Schwan, Adrian L.
Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K
title Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K
title_full Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K
title_fullStr Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K
title_full_unstemmed Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K
title_short Triclinic modification of N-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 120 (1) K
title_sort triclinic modification of n-[(1,1-di­methyl­ethoxy)carbon­yl]-3-[(r)-prop-2-en-1-ylsulfin­yl]-(r)-alanine ethyl ester at 120 (1) k
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969554/
https://www.ncbi.nlm.nih.gov/pubmed/21583234
http://dx.doi.org/10.1107/S1600536809019011
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