N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate

The title compound, C(16)H(16)N(2)O(6)·C(2)H(5)OH, was synthesized from 3,4,5-trihydroxy­benzoyl­hydrazide and 2,4-dimethoxy­benzaldehyde in ethanol. The compound is not planar, with the two aromatic planes of the two aromatic rings twisted by 15.6 (1)°. The hydr­oxy groups are involved in both intr...

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Detalles Bibliográficos
Autores principales: Alhadi, Abeer A., Saharin, Siti Munirah, Mohd Ali, Hapipah, Robinson, Ward T., Abdulla, Mahmood A.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969598/
https://www.ncbi.nlm.nih.gov/pubmed/21583222
http://dx.doi.org/10.1107/S1600536809018947
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author Alhadi, Abeer A.
Saharin, Siti Munirah
Mohd Ali, Hapipah
Robinson, Ward T.
Abdulla, Mahmood A.
author_facet Alhadi, Abeer A.
Saharin, Siti Munirah
Mohd Ali, Hapipah
Robinson, Ward T.
Abdulla, Mahmood A.
author_sort Alhadi, Abeer A.
collection PubMed
description The title compound, C(16)H(16)N(2)O(6)·C(2)H(5)OH, was synthesized from 3,4,5-trihydroxy­benzoyl­hydrazide and 2,4-dimethoxy­benzaldehyde in ethanol. The compound is not planar, with the two aromatic planes of the two aromatic rings twisted by 15.6 (1)°. The hydr­oxy groups are involved in both intra­molecular O—H⋯O and inter­molecular O—H⋯N and O—H⋯O hydrogen bonds and a C—H⋯O interaction also occurs.
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spelling pubmed-29695982010-12-30 N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate Alhadi, Abeer A. Saharin, Siti Munirah Mohd Ali, Hapipah Robinson, Ward T. Abdulla, Mahmood A. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(16)H(16)N(2)O(6)·C(2)H(5)OH, was synthesized from 3,4,5-trihydroxy­benzoyl­hydrazide and 2,4-dimethoxy­benzaldehyde in ethanol. The compound is not planar, with the two aromatic planes of the two aromatic rings twisted by 15.6 (1)°. The hydr­oxy groups are involved in both intra­molecular O—H⋯O and inter­molecular O—H⋯N and O—H⋯O hydrogen bonds and a C—H⋯O interaction also occurs. International Union of Crystallography 2009-05-23 /pmc/articles/PMC2969598/ /pubmed/21583222 http://dx.doi.org/10.1107/S1600536809018947 Text en © Alhadi et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Alhadi, Abeer A.
Saharin, Siti Munirah
Mohd Ali, Hapipah
Robinson, Ward T.
Abdulla, Mahmood A.
N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
title N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
title_full N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
title_fullStr N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
title_full_unstemmed N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
title_short N′-(2,4-Dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
title_sort n′-(2,4-dimethoxy­benzyl­idene)-3,4,5-trihydroxy­benzohydrazide ethanol solvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969598/
https://www.ncbi.nlm.nih.gov/pubmed/21583222
http://dx.doi.org/10.1107/S1600536809018947
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