5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine

The title compound, C(7)H(6)N(4)S, was synthesized by reacting pyridine-3-carboxylic acid and thio­semicarbazide. The dihedral angle between the planes of the thia­diazole and pyridine rings is 32.42 (14)°. In the crystal structure, inter­molecular N—H⋯N inter­actions link the mol­ecules into a thre...

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Detalles Bibliográficos
Autores principales: Wang, Yao, Wan, Rong, Han, Feng, Wang, Peng
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969629/
https://www.ncbi.nlm.nih.gov/pubmed/21583285
http://dx.doi.org/10.1107/S1600536809019564
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author Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
author_facet Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
author_sort Wang, Yao
collection PubMed
description The title compound, C(7)H(6)N(4)S, was synthesized by reacting pyridine-3-carboxylic acid and thio­semicarbazide. The dihedral angle between the planes of the thia­diazole and pyridine rings is 32.42 (14)°. In the crystal structure, inter­molecular N—H⋯N inter­actions link the mol­ecules into a three-dimensional network, forming R (2) (2)(8) ring motifs. π–π contacts between thia­diazole rings [centroid–centroid distance = 3.666 (1) Å] may further stabilize the structure.
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spelling pubmed-29696292010-12-30 5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine Wang, Yao Wan, Rong Han, Feng Wang, Peng Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(7)H(6)N(4)S, was synthesized by reacting pyridine-3-carboxylic acid and thio­semicarbazide. The dihedral angle between the planes of the thia­diazole and pyridine rings is 32.42 (14)°. In the crystal structure, inter­molecular N—H⋯N inter­actions link the mol­ecules into a three-dimensional network, forming R (2) (2)(8) ring motifs. π–π contacts between thia­diazole rings [centroid–centroid distance = 3.666 (1) Å] may further stabilize the structure. International Union of Crystallography 2009-05-29 /pmc/articles/PMC2969629/ /pubmed/21583285 http://dx.doi.org/10.1107/S1600536809019564 Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Yao
Wan, Rong
Han, Feng
Wang, Peng
5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title 5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_full 5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_fullStr 5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_full_unstemmed 5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_short 5-(3-Pyrid­yl)-1,3,4-thia­diazol-2-amine
title_sort 5-(3-pyrid­yl)-1,3,4-thia­diazol-2-amine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969629/
https://www.ncbi.nlm.nih.gov/pubmed/21583285
http://dx.doi.org/10.1107/S1600536809019564
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AT wanrong 53pyridyl134thiadiazol2amine
AT hanfeng 53pyridyl134thiadiazol2amine
AT wangpeng 53pyridyl134thiadiazol2amine

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