1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)

The title compound, 3C(14)H(12)N(2)O(2)·C(3)H(7)NO, was synthesized by reaction of benzoyl chloride with hydrazine hydrate under microwave irradition. The asymmetric unit comprises three 1,2-dibenzoyl­hydrazine mol­ecules and one dimethyl­formamide mol­ecule. The 1,2-dibenzoyl­hydrazine mol­ecules a...

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Detalles Bibliográficos
Autores principales: He, Qing-Peng, Li, Hong-Gang, Wang, Guang-Bo, Fu, Feng-Lian, Liu, Ming-Shi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969677/
https://www.ncbi.nlm.nih.gov/pubmed/21583131
http://dx.doi.org/10.1107/S1600536809016778
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author He, Qing-Peng
Li, Hong-Gang
Wang, Guang-Bo
Fu, Feng-Lian
Liu, Ming-Shi
author_facet He, Qing-Peng
Li, Hong-Gang
Wang, Guang-Bo
Fu, Feng-Lian
Liu, Ming-Shi
author_sort He, Qing-Peng
collection PubMed
description The title compound, 3C(14)H(12)N(2)O(2)·C(3)H(7)NO, was synthesized by reaction of benzoyl chloride with hydrazine hydrate under microwave irradition. The asymmetric unit comprises three 1,2-dibenzoyl­hydrazine mol­ecules and one dimethyl­formamide mol­ecule. The 1,2-dibenzoyl­hydrazine mol­ecules are linked by pairs of N—H⋯O hydrogen bonds into chains propagating along [010].
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spelling pubmed-29696772010-12-30 1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1) He, Qing-Peng Li, Hong-Gang Wang, Guang-Bo Fu, Feng-Lian Liu, Ming-Shi Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, 3C(14)H(12)N(2)O(2)·C(3)H(7)NO, was synthesized by reaction of benzoyl chloride with hydrazine hydrate under microwave irradition. The asymmetric unit comprises three 1,2-dibenzoyl­hydrazine mol­ecules and one dimethyl­formamide mol­ecule. The 1,2-dibenzoyl­hydrazine mol­ecules are linked by pairs of N—H⋯O hydrogen bonds into chains propagating along [010]. International Union of Crystallography 2009-05-14 /pmc/articles/PMC2969677/ /pubmed/21583131 http://dx.doi.org/10.1107/S1600536809016778 Text en © He et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
He, Qing-Peng
Li, Hong-Gang
Wang, Guang-Bo
Fu, Feng-Lian
Liu, Ming-Shi
1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)
title 1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)
title_full 1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)
title_fullStr 1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)
title_full_unstemmed 1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)
title_short 1,2-Dibenzoyl­hydrazine–dimethyl­formamide (3/1)
title_sort 1,2-dibenzoyl­hydrazine–dimethyl­formamide (3/1)
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969677/
https://www.ncbi.nlm.nih.gov/pubmed/21583131
http://dx.doi.org/10.1107/S1600536809016778
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AT lihonggang 12dibenzoylhydrazinedimethylformamide31
AT wangguangbo 12dibenzoylhydrazinedimethylformamide31
AT fufenglian 12dibenzoylhydrazinedimethylformamide31
AT liumingshi 12dibenzoylhydrazinedimethylformamide31

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