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Ethyl 2-amino-4-(3-chlorophenyl)-5,10-dioxo-5,10-dihydro-4H-benzo[g]chromene-3-carboxylate
The title molecule, C(22)H(16)ClNO(5), was obtained by the reaction of (E)-ethyl 3-(3-chlorophenyl)-2-cyanoacrylate and 2-hydroxynaphthalene-1,4-dione catalysed by triethylamine in ethanol. In the crystal structure, the chlorobenzene ring makes a dihedral angle of 88.63 (4)° with the fused ring...
Autores principales: | , , |
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Formato: | Texto |
Lenguaje: | English |
Publicado: |
International Union of Crystallography
2009
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Materias: | |
Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969697/ https://www.ncbi.nlm.nih.gov/pubmed/21583179 http://dx.doi.org/10.1107/S160053680901753X |
Sumario: | The title molecule, C(22)H(16)ClNO(5), was obtained by the reaction of (E)-ethyl 3-(3-chlorophenyl)-2-cyanoacrylate and 2-hydroxynaphthalene-1,4-dione catalysed by triethylamine in ethanol. In the crystal structure, the chlorobenzene ring makes a dihedral angle of 88.63 (4)° with the fused ring system. The six-membered ring formed by an intramolecular N—H⋯O hydrogen bond is almost planar. The crystal packing is stabilized by N—H⋯O hydrogen bonds. |
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