2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione

In the title mol­ecule, C(24)H(28)N(6)O(2)S(2), the dihedral angle between the aromatic ring planes is 42.2 (1)°. In the crystal structure, the hydr­oxy groups are involved in O—H⋯S hydrogen bonding, which links the mol­ecules into corrugated layers propagating parallel to the bc plane.

Detalles Bibliográficos
Autores principales: Wang, Zihua, Xi, Hailing
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969711/
https://www.ncbi.nlm.nih.gov/pubmed/21583267
http://dx.doi.org/10.1107/S1600536809019230
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author Wang, Zihua
Xi, Hailing
author_facet Wang, Zihua
Xi, Hailing
author_sort Wang, Zihua
collection PubMed
description In the title mol­ecule, C(24)H(28)N(6)O(2)S(2), the dihedral angle between the aromatic ring planes is 42.2 (1)°. In the crystal structure, the hydr­oxy groups are involved in O—H⋯S hydrogen bonding, which links the mol­ecules into corrugated layers propagating parallel to the bc plane.
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spelling pubmed-29697112010-12-30 2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione Wang, Zihua Xi, Hailing Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title mol­ecule, C(24)H(28)N(6)O(2)S(2), the dihedral angle between the aromatic ring planes is 42.2 (1)°. In the crystal structure, the hydr­oxy groups are involved in O—H⋯S hydrogen bonding, which links the mol­ecules into corrugated layers propagating parallel to the bc plane. International Union of Crystallography 2009-05-29 /pmc/articles/PMC2969711/ /pubmed/21583267 http://dx.doi.org/10.1107/S1600536809019230 Text en © Wang and Xi 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Zihua
Xi, Hailing
2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title 2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_full 2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_fullStr 2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_full_unstemmed 2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_short 2,6-Bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
title_sort 2,6-bis(2-hydroxy­ethyl)-8b,8c-diphenyl­perhydro-2,3a,4a,6,7a,8a-hexa­azacyclo­penta­[def]fluorene-4,8-dithione
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969711/
https://www.ncbi.nlm.nih.gov/pubmed/21583267
http://dx.doi.org/10.1107/S1600536809019230
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AT xihailing 26bis2hydroxyethyl8b8cdiphenylperhydro23a4a67a8ahexaazacyclopentadeffluorene48dithione

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