9-O-Butyl­berberrubinium bromide

In the title compound, C(23)H(24)NO(4) (+)·Br(−), the butyl chain is disordered between two conformations; the occupancies refined to 0.735 (7) and 0.265 (7). The dihedral angle between the naphthalene ring system and the phenyl ring is 11.6 (2)°. In the crystal structure, the cations are packed via...

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Detalles Bibliográficos
Autores principales: Chen, Zhu, Li, Xue-Gang, Xie, Yong-Sheng, Ye, Xiao-Li
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969731/
https://www.ncbi.nlm.nih.gov/pubmed/21583219
http://dx.doi.org/10.1107/S1600536809018388
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author Chen, Zhu
Li, Xue-Gang
Xie, Yong-Sheng
Ye, Xiao-Li
author_facet Chen, Zhu
Li, Xue-Gang
Xie, Yong-Sheng
Ye, Xiao-Li
author_sort Chen, Zhu
collection PubMed
description In the title compound, C(23)H(24)NO(4) (+)·Br(−), the butyl chain is disordered between two conformations; the occupancies refined to 0.735 (7) and 0.265 (7). The dihedral angle between the naphthalene ring system and the phenyl ring is 11.6 (2)°. In the crystal structure, the cations are packed via π–π inter­actions into stacks propagating in the [010] direction. Weak inter­molecular C—H⋯O and C—H⋯Br hydrogen bonds contribute further to the crystal packing stability.
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spelling pubmed-29697312010-12-30 9-O-Butyl­berberrubinium bromide Chen, Zhu Li, Xue-Gang Xie, Yong-Sheng Ye, Xiao-Li Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(23)H(24)NO(4) (+)·Br(−), the butyl chain is disordered between two conformations; the occupancies refined to 0.735 (7) and 0.265 (7). The dihedral angle between the naphthalene ring system and the phenyl ring is 11.6 (2)°. In the crystal structure, the cations are packed via π–π inter­actions into stacks propagating in the [010] direction. Weak inter­molecular C—H⋯O and C—H⋯Br hydrogen bonds contribute further to the crystal packing stability. International Union of Crystallography 2009-05-23 /pmc/articles/PMC2969731/ /pubmed/21583219 http://dx.doi.org/10.1107/S1600536809018388 Text en © Chen et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Chen, Zhu
Li, Xue-Gang
Xie, Yong-Sheng
Ye, Xiao-Li
9-O-Butyl­berberrubinium bromide
title 9-O-Butyl­berberrubinium bromide
title_full 9-O-Butyl­berberrubinium bromide
title_fullStr 9-O-Butyl­berberrubinium bromide
title_full_unstemmed 9-O-Butyl­berberrubinium bromide
title_short 9-O-Butyl­berberrubinium bromide
title_sort 9-o-butyl­berberrubinium bromide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969731/
https://www.ncbi.nlm.nih.gov/pubmed/21583219
http://dx.doi.org/10.1107/S1600536809018388
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AT lixuegang 9obutylberberrubiniumbromide
AT xieyongsheng 9obutylberberrubiniumbromide
AT yexiaoli 9obutylberberrubiniumbromide

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