Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K

In the monoclinic polymorph of the title compound, C(13)H(23)NO(5)S, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into one-dimensional chains along [100]. The atoms of the terminal propenyl group are disordered over two sets of sites with refined occupancies of 0.69 (2) and 0.31 (2)....

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Detalles Bibliográficos
Autores principales: Singh, Suneel P., Verdu, Marcus J., Lough, Alan J., Schwan, Adrian L.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969828/
https://www.ncbi.nlm.nih.gov/pubmed/21583233
http://dx.doi.org/10.1107/S1600536809019023
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author Singh, Suneel P.
Verdu, Marcus J.
Lough, Alan J.
Schwan, Adrian L.
author_facet Singh, Suneel P.
Verdu, Marcus J.
Lough, Alan J.
Schwan, Adrian L.
author_sort Singh, Suneel P.
collection PubMed
description In the monoclinic polymorph of the title compound, C(13)H(23)NO(5)S, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into one-dimensional chains along [100]. The atoms of the terminal propenyl group are disordered over two sets of sites with refined occupancies of 0.69 (2) and 0.31 (2).
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spelling pubmed-29698282010-12-30 Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K Singh, Suneel P. Verdu, Marcus J. Lough, Alan J. Schwan, Adrian L. Acta Crystallogr Sect E Struct Rep Online Organic Papers In the monoclinic polymorph of the title compound, C(13)H(23)NO(5)S, inter­molecular N—H⋯O hydrogen bonds link mol­ecules into one-dimensional chains along [100]. The atoms of the terminal propenyl group are disordered over two sets of sites with refined occupancies of 0.69 (2) and 0.31 (2). International Union of Crystallography 2009-05-23 /pmc/articles/PMC2969828/ /pubmed/21583233 http://dx.doi.org/10.1107/S1600536809019023 Text en © Singh et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Singh, Suneel P.
Verdu, Marcus J.
Lough, Alan J.
Schwan, Adrian L.
Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K
title Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K
title_full Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K
title_fullStr Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K
title_full_unstemmed Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K
title_short Monoclinic modification of N-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(R)-prop-2-en-1-ylsulfin­yl]-(R)-alanine ethyl ester at 200 (1) K
title_sort monoclinic modification of n-[(1,1-dimethyl­ethoxy)carbon­yl]-3-[(r)-prop-2-en-1-ylsulfin­yl]-(r)-alanine ethyl ester at 200 (1) k
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969828/
https://www.ncbi.nlm.nih.gov/pubmed/21583233
http://dx.doi.org/10.1107/S1600536809019023
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