9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one

The title compound, C(25)H(22)N(2)O(3), was synthesized by the reaction of 3-nitro­benzaldehyde, dimedone and 2-naphthyl­amine in ethanol. In the mol­ecular structure, the cyclo­hexenone ring adopts an envelope conformation, whereas the piperidine ring has a boat conformation. The crystal packing is...

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Detalles Bibliográficos
Autores principales: Jia, Runhong, Peng, Juhua, Tu, Shujiang
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969871/
https://www.ncbi.nlm.nih.gov/pubmed/21577677
http://dx.doi.org/10.1107/S1600536809033935
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author Jia, Runhong
Peng, Juhua
Tu, Shujiang
author_facet Jia, Runhong
Peng, Juhua
Tu, Shujiang
author_sort Jia, Runhong
collection PubMed
description The title compound, C(25)H(22)N(2)O(3), was synthesized by the reaction of 3-nitro­benzaldehyde, dimedone and 2-naphthyl­amine in ethanol. In the mol­ecular structure, the cyclo­hexenone ring adopts an envelope conformation, whereas the piperidine ring has a boat conformation. The crystal packing is stabilized by inter­molecular N—H⋯O hydrogen bonds.
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spelling pubmed-29698712010-12-30 9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one Jia, Runhong Peng, Juhua Tu, Shujiang Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(25)H(22)N(2)O(3), was synthesized by the reaction of 3-nitro­benzaldehyde, dimedone and 2-naphthyl­amine in ethanol. In the mol­ecular structure, the cyclo­hexenone ring adopts an envelope conformation, whereas the piperidine ring has a boat conformation. The crystal packing is stabilized by inter­molecular N—H⋯O hydrogen bonds. International Union of Crystallography 2009-08-29 /pmc/articles/PMC2969871/ /pubmed/21577677 http://dx.doi.org/10.1107/S1600536809033935 Text en © Jia et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jia, Runhong
Peng, Juhua
Tu, Shujiang
9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
title 9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
title_full 9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
title_fullStr 9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
title_full_unstemmed 9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
title_short 9,9-Dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
title_sort 9,9-dimethyl-12-(3-nitro­phen­yl)-7,8,9,10,11,12-hexa­hydro­benz[a]acridin-11-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969871/
https://www.ncbi.nlm.nih.gov/pubmed/21577677
http://dx.doi.org/10.1107/S1600536809033935
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AT pengjuhua 99dimethyl123nitrophenyl789101112hexahydrobenzaacridin11one
AT tushujiang 99dimethyl123nitrophenyl789101112hexahydrobenzaacridin11one

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