7α,15α-Dibromo-8,16-diphenyl-6,7,14,15-tetra­hydro-6α,14α-epithio­cyclo­octa­[1,2-b:5,6-b′]diquinoline deuterochloro­form solvate

In the racemic title compound, C(34)H(22)Br(2)N(2)S·CDCl(3), pairs of diquinoline host mol­ecules form centrosymmetric brick-like dimers utilizing three different aryl edge-to-face inter­actions (EF(1–3)). The dimeric (EF)(6) (i.e. 2 × EF(1–3)) building blocks pack with the deuterochloro­form guest...

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Detalles Bibliográficos
Autores principales: Chan, Isa Y. H., Bishop, Roger, Craig, Donald C., Bhadbhade, Mohan M., Scudder, Marcia L.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969924/
https://www.ncbi.nlm.nih.gov/pubmed/21577650
http://dx.doi.org/10.1107/S1600536809032978
Descripción
Sumario:In the racemic title compound, C(34)H(22)Br(2)N(2)S·CDCl(3), pairs of diquinoline host mol­ecules form centrosymmetric brick-like dimers utilizing three different aryl edge-to-face inter­actions (EF(1–3)). The dimeric (EF)(6) (i.e. 2 × EF(1–3)) building blocks pack with the deuterochloro­form guest mol­ecules positioned near each of their corners. The Cl atoms of the latter are disordered over two sets of sites in a 0.53 (2):0.47 (2) ratio.

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