(E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide

The title compound, C(14)H(9)BrCl(2)N(2)O, was synthesized by the reaction of 2,4-dichloro­benzaldehyde with an equimolar quantity of 3-bromo­benzohydrazide in methanol. The mol­ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 5.3 (2)°. In the...

Descripción completa

Detalles Bibliográficos
Autor principal: Cao, Guo-Biao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969972/
https://www.ncbi.nlm.nih.gov/pubmed/21577503
http://dx.doi.org/10.1107/S1600536809030220
_version_ 1782190311228833792
author Cao, Guo-Biao
author_facet Cao, Guo-Biao
author_sort Cao, Guo-Biao
collection PubMed
description The title compound, C(14)H(9)BrCl(2)N(2)O, was synthesized by the reaction of 2,4-dichloro­benzaldehyde with an equimolar quantity of 3-bromo­benzohydrazide in methanol. The mol­ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 5.3 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and C—H⋯O hydrogen bonds, forming chains running along the c axis.
format Text
id pubmed-2969972
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29699722010-12-30 (E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide Cao, Guo-Biao Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(9)BrCl(2)N(2)O, was synthesized by the reaction of 2,4-dichloro­benzaldehyde with an equimolar quantity of 3-bromo­benzohydrazide in methanol. The mol­ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 5.3 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and C—H⋯O hydrogen bonds, forming chains running along the c axis. International Union of Crystallography 2009-08-08 /pmc/articles/PMC2969972/ /pubmed/21577503 http://dx.doi.org/10.1107/S1600536809030220 Text en © Guo-Biao Cao 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Cao, Guo-Biao
(E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide
title (E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide
title_full (E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide
title_fullStr (E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide
title_full_unstemmed (E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide
title_short (E)-3-Bromo-N′-(2,4-dichloro­benzyl­idene)benzohydrazide
title_sort (e)-3-bromo-n′-(2,4-dichloro­benzyl­idene)benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2969972/
https://www.ncbi.nlm.nih.gov/pubmed/21577503
http://dx.doi.org/10.1107/S1600536809030220
work_keys_str_mv AT caoguobiao e3bromon24dichlorobenzylidenebenzohydrazide

Ejemplares similares