2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one

The title compound, C(14)H(11)ClN(2)O, was synthesized by the reaction of 2-chloro­benzaldehyde and 2-amino­benzamide in an ionic liquid. The pyrimidine ring adopts a skew-boat conformation and the two benzene rings make a dihedral angle of 87.1 (1)°. In the crystal, N—H⋯O and C—H⋯N hydrogen bonding...

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Detalles Bibliográficos
Autores principales: Li, Ming-Jian, Feng, Chang-Jun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970036/
https://www.ncbi.nlm.nih.gov/pubmed/21577554
http://dx.doi.org/10.1107/S1600536809031328
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author Li, Ming-Jian
Feng, Chang-Jun
author_facet Li, Ming-Jian
Feng, Chang-Jun
author_sort Li, Ming-Jian
collection PubMed
description The title compound, C(14)H(11)ClN(2)O, was synthesized by the reaction of 2-chloro­benzaldehyde and 2-amino­benzamide in an ionic liquid. The pyrimidine ring adopts a skew-boat conformation and the two benzene rings make a dihedral angle of 87.1 (1)°. In the crystal, N—H⋯O and C—H⋯N hydrogen bonding links the mol­ecules along b.
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spelling pubmed-29700362010-12-30 2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one Li, Ming-Jian Feng, Chang-Jun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(11)ClN(2)O, was synthesized by the reaction of 2-chloro­benzaldehyde and 2-amino­benzamide in an ionic liquid. The pyrimidine ring adopts a skew-boat conformation and the two benzene rings make a dihedral angle of 87.1 (1)°. In the crystal, N—H⋯O and C—H⋯N hydrogen bonding links the mol­ecules along b. International Union of Crystallography 2009-08-15 /pmc/articles/PMC2970036/ /pubmed/21577554 http://dx.doi.org/10.1107/S1600536809031328 Text en © Li and Feng 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Ming-Jian
Feng, Chang-Jun
2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one
title 2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one
title_full 2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one
title_fullStr 2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one
title_full_unstemmed 2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one
title_short 2-(2-Chloro­phen­yl)-2,3-dihydro­quinazolin-4(1H)-one
title_sort 2-(2-chloro­phen­yl)-2,3-dihydro­quinazolin-4(1h)-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970036/
https://www.ncbi.nlm.nih.gov/pubmed/21577554
http://dx.doi.org/10.1107/S1600536809031328
work_keys_str_mv AT limingjian 22chlorophenyl23dihydroquinazolin41hone
AT fengchangjun 22chlorophenyl23dihydroquinazolin41hone

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