1,2-Bis(4-nitro­benzo­yl)hydrazine

The title mol­ecule, C(14)H(10)N(4)O(6), crystallizes with one half-mol­ecule in the asymmetric unit; the mid-point of the N—N bond lies on an inversion centre. The nitro and amide groups are twisted with respect to the benzene ring, making dihedral angles of 14.6 (5) and 31.1 (5)°, respectively. In...

Descripción completa

Detalles Bibliográficos
Autores principales: Jiang, Xue-Yue, Feng, Xiao-Jun, Yang, Song, Xu, Hua-Jie, Hao, Ling-Yun
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970062/
https://www.ncbi.nlm.nih.gov/pubmed/21577593
http://dx.doi.org/10.1107/S160053680903181X
_version_ 1782190335227592704
author Jiang, Xue-Yue
Feng, Xiao-Jun
Yang, Song
Xu, Hua-Jie
Hao, Ling-Yun
author_facet Jiang, Xue-Yue
Feng, Xiao-Jun
Yang, Song
Xu, Hua-Jie
Hao, Ling-Yun
author_sort Jiang, Xue-Yue
collection PubMed
description The title mol­ecule, C(14)H(10)N(4)O(6), crystallizes with one half-mol­ecule in the asymmetric unit; the mid-point of the N—N bond lies on an inversion centre. The nitro and amide groups are twisted with respect to the benzene ring, making dihedral angles of 14.6 (5) and 31.1 (5)°, respectively. In the crystal structure, mol­ecules are linked through N—H⋯O hydrogen bonding between the imino and carbonyl groups.
format Text
id pubmed-2970062
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29700622010-12-30 1,2-Bis(4-nitro­benzo­yl)hydrazine Jiang, Xue-Yue Feng, Xiao-Jun Yang, Song Xu, Hua-Jie Hao, Ling-Yun Acta Crystallogr Sect E Struct Rep Online Organic Papers The title mol­ecule, C(14)H(10)N(4)O(6), crystallizes with one half-mol­ecule in the asymmetric unit; the mid-point of the N—N bond lies on an inversion centre. The nitro and amide groups are twisted with respect to the benzene ring, making dihedral angles of 14.6 (5) and 31.1 (5)°, respectively. In the crystal structure, mol­ecules are linked through N—H⋯O hydrogen bonding between the imino and carbonyl groups. International Union of Crystallography 2009-08-19 /pmc/articles/PMC2970062/ /pubmed/21577593 http://dx.doi.org/10.1107/S160053680903181X Text en © Jiang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Jiang, Xue-Yue
Feng, Xiao-Jun
Yang, Song
Xu, Hua-Jie
Hao, Ling-Yun
1,2-Bis(4-nitro­benzo­yl)hydrazine
title 1,2-Bis(4-nitro­benzo­yl)hydrazine
title_full 1,2-Bis(4-nitro­benzo­yl)hydrazine
title_fullStr 1,2-Bis(4-nitro­benzo­yl)hydrazine
title_full_unstemmed 1,2-Bis(4-nitro­benzo­yl)hydrazine
title_short 1,2-Bis(4-nitro­benzo­yl)hydrazine
title_sort 1,2-bis(4-nitro­benzo­yl)hydrazine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970062/
https://www.ncbi.nlm.nih.gov/pubmed/21577593
http://dx.doi.org/10.1107/S160053680903181X
work_keys_str_mv AT jiangxueyue 12bis4nitrobenzoylhydrazine
AT fengxiaojun 12bis4nitrobenzoylhydrazine
AT yangsong 12bis4nitrobenzoylhydrazine
AT xuhuajie 12bis4nitrobenzoylhydrazine
AT haolingyun 12bis4nitrobenzoylhydrazine

Ejemplares similares