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o-Toluenesulfonamide: a redetermination
The structure of the title compound, C(7)H(9)NO(2)S, was previously determined from powder diffraction data [Tremayne, Seaton & Glidewell (2002). Acta Cryst. B58, 823–834]. It has now been refined to a significantly higher precision. The amino N-atom is bent with a C—C—S—N torsion angle of −65.8...
| Autores principales: | , , , |
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| Formato: | Texto |
| Lenguaje: | English |
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International Union of Crystallography
2009
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| Acceso en línea: | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970068/ https://www.ncbi.nlm.nih.gov/pubmed/21577654 http://dx.doi.org/10.1107/S1600536809033686 |
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| author | Gowda, B. Thimme Foro, Sabine Shakuntala, K. Fuess, Hartmut |
| author_facet | Gowda, B. Thimme Foro, Sabine Shakuntala, K. Fuess, Hartmut |
| author_sort | Gowda, B. Thimme |
| collection | PubMed |
| description | The structure of the title compound, C(7)H(9)NO(2)S, was previously determined from powder diffraction data [Tremayne, Seaton & Glidewell (2002). Acta Cryst. B58, 823–834]. It has now been refined to a significantly higher precision. The amino N-atom is bent with a C—C—S—N torsion angle of −65.8 (2)deg;. In the crystal, molecules are packed into a three-dimensional framework/supramolecular structure through hydrogen bonds between the two H atoms of the sulfonamide group and sulfonyl O atoms of neighbouring molecules. |
| format | Text |
| id | pubmed-2970068 |
| institution | National Center for Biotechnology Information |
| language | English |
| publishDate | 2009 |
| publisher | International Union of Crystallography |
| record_format | MEDLINE/PubMed |
| spelling | pubmed-29700682010-12-30 o-Toluenesulfonamide: a redetermination Gowda, B. Thimme Foro, Sabine Shakuntala, K. Fuess, Hartmut Acta Crystallogr Sect E Struct Rep Online Organic Papers The structure of the title compound, C(7)H(9)NO(2)S, was previously determined from powder diffraction data [Tremayne, Seaton & Glidewell (2002). Acta Cryst. B58, 823–834]. It has now been refined to a significantly higher precision. The amino N-atom is bent with a C—C—S—N torsion angle of −65.8 (2)deg;. In the crystal, molecules are packed into a three-dimensional framework/supramolecular structure through hydrogen bonds between the two H atoms of the sulfonamide group and sulfonyl O atoms of neighbouring molecules. International Union of Crystallography 2009-08-29 /pmc/articles/PMC2970068/ /pubmed/21577654 http://dx.doi.org/10.1107/S1600536809033686 Text en © Gowda et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited. |
| spellingShingle | Organic Papers Gowda, B. Thimme Foro, Sabine Shakuntala, K. Fuess, Hartmut o-Toluenesulfonamide: a redetermination |
| title |
o-Toluenesulfonamide: a redetermination |
| title_full |
o-Toluenesulfonamide: a redetermination |
| title_fullStr |
o-Toluenesulfonamide: a redetermination |
| title_full_unstemmed |
o-Toluenesulfonamide: a redetermination |
| title_short |
o-Toluenesulfonamide: a redetermination |
| title_sort | o-toluenesulfonamide: a redetermination |
| topic | Organic Papers |
| url | https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970068/ https://www.ncbi.nlm.nih.gov/pubmed/21577654 http://dx.doi.org/10.1107/S1600536809033686 |
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