2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate

In the title salt, C(15)H(17)N(2) (+)·ClO(4) (−), the isoindoline N atom is protonated and an intra­molecular N—H⋯N hydrogen bond occurs. In the crystal, N—H⋯O and numerous weak C—H⋯O inter­actions occur between the cation and anion. The O atoms of the perchlorate anion are disordered over four sets...

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Detalles Bibliográficos
Autores principales: Butcher, Ray J., Tesema, Yohannes T., Yisgedu, Teshome B., Gultneh, Yilma
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970132/
https://www.ncbi.nlm.nih.gov/pubmed/21577581
http://dx.doi.org/10.1107/S1600536809032024
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author Butcher, Ray J.
Tesema, Yohannes T.
Yisgedu, Teshome B.
Gultneh, Yilma
author_facet Butcher, Ray J.
Tesema, Yohannes T.
Yisgedu, Teshome B.
Gultneh, Yilma
author_sort Butcher, Ray J.
collection PubMed
description In the title salt, C(15)H(17)N(2) (+)·ClO(4) (−), the isoindoline N atom is protonated and an intra­molecular N—H⋯N hydrogen bond occurs. In the crystal, N—H⋯O and numerous weak C—H⋯O inter­actions occur between the cation and anion. The O atoms of the perchlorate anion are disordered over four sets of sites with occupancies of 0.438 (4), 0.270 (9), 0.155 (8) and 0.138 (5).
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spelling pubmed-29701322010-12-30 2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate Butcher, Ray J. Tesema, Yohannes T. Yisgedu, Teshome B. Gultneh, Yilma Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title salt, C(15)H(17)N(2) (+)·ClO(4) (−), the isoindoline N atom is protonated and an intra­molecular N—H⋯N hydrogen bond occurs. In the crystal, N—H⋯O and numerous weak C—H⋯O inter­actions occur between the cation and anion. The O atoms of the perchlorate anion are disordered over four sets of sites with occupancies of 0.438 (4), 0.270 (9), 0.155 (8) and 0.138 (5). International Union of Crystallography 2009-08-19 /pmc/articles/PMC2970132/ /pubmed/21577581 http://dx.doi.org/10.1107/S1600536809032024 Text en © Butcher et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Butcher, Ray J.
Tesema, Yohannes T.
Yisgedu, Teshome B.
Gultneh, Yilma
2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate
title 2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate
title_full 2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate
title_fullStr 2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate
title_full_unstemmed 2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate
title_short 2-[2-(2-Pyrid­yl)eth­yl]isoindolinium perchlorate
title_sort 2-[2-(2-pyrid­yl)eth­yl]isoindolinium perchlorate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970132/
https://www.ncbi.nlm.nih.gov/pubmed/21577581
http://dx.doi.org/10.1107/S1600536809032024
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AT yisgeduteshomeb 222pyridylethylisoindoliniumperchlorate
AT gultnehyilma 222pyridylethylisoindoliniumperchlorate

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