(E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide

The title compound, C(14)H(10)ClN(3)O(4), was synthesized by the reaction of 5-hydr­oxy-2-nitro­benzaldehyde with an equimolar quantity of 4-chloro­benzohydrazide in methanol. The mol­ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 3.9 (2)°....

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Detalles Bibliográficos
Autor principal: Cao, Guo-Biao
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970190/
https://www.ncbi.nlm.nih.gov/pubmed/21577874
http://dx.doi.org/10.1107/S1600536809035740
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author Cao, Guo-Biao
author_facet Cao, Guo-Biao
author_sort Cao, Guo-Biao
collection PubMed
description The title compound, C(14)H(10)ClN(3)O(4), was synthesized by the reaction of 5-hydr­oxy-2-nitro­benzaldehyde with an equimolar quantity of 4-chloro­benzohydrazide in methanol. The mol­ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 3.9 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds, forming chains running along the b axis.
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spelling pubmed-29701902010-12-30 (E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide Cao, Guo-Biao Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(10)ClN(3)O(4), was synthesized by the reaction of 5-hydr­oxy-2-nitro­benzaldehyde with an equimolar quantity of 4-chloro­benzohydrazide in methanol. The mol­ecule displays an E configuration about the C=N bond. The dihedral angle between the two benzene rings is 3.9 (2)°. In the crystal structure, mol­ecules are linked through inter­molecular N—H⋯O and O—H⋯O hydrogen bonds, forming chains running along the b axis. International Union of Crystallography 2009-09-09 /pmc/articles/PMC2970190/ /pubmed/21577874 http://dx.doi.org/10.1107/S1600536809035740 Text en © Guo-Biao Cao 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Cao, Guo-Biao
(E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
title (E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
title_full (E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
title_fullStr (E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
title_full_unstemmed (E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
title_short (E)-4-Chloro-N′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
title_sort (e)-4-chloro-n′-(5-hydr­oxy-2-nitro­benzyl­idene)benzohydrazide
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970190/
https://www.ncbi.nlm.nih.gov/pubmed/21577874
http://dx.doi.org/10.1107/S1600536809035740
work_keys_str_mv AT caoguobiao e4chloron5hydroxy2nitrobenzylidenebenzohydrazide

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