2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine

In the title structure, C(18)H(20)N(4), the aromatic rings are almost orthogonal [81.6 (2)°]. The mol­ecule has symmetry 2 since it is situated on a crystallographic twofold axis. There are only weak inter­molecular inter­actions present in the structure, notably C—H⋯π-electron ring inter­actions. T...

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Detalles Bibliográficos
Autores principales: Rivera, Augusto, Maldonado, Mauricio, Ríos-Motta, Jaime, González-Salas, Diego, Dacunha-Marinho, Bruno
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970222/
https://www.ncbi.nlm.nih.gov/pubmed/21577994
http://dx.doi.org/10.1107/S1600536809038380
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author Rivera, Augusto
Maldonado, Mauricio
Ríos-Motta, Jaime
González-Salas, Diego
Dacunha-Marinho, Bruno
author_facet Rivera, Augusto
Maldonado, Mauricio
Ríos-Motta, Jaime
González-Salas, Diego
Dacunha-Marinho, Bruno
author_sort Rivera, Augusto
collection PubMed
description In the title structure, C(18)H(20)N(4), the aromatic rings are almost orthogonal [81.6 (2)°]. The mol­ecule has symmetry 2 since it is situated on a crystallographic twofold axis. There are only weak inter­molecular inter­actions present in the structure, notably C—H⋯π-electron ring inter­actions. The (1)H and (13)C NMR spectra are in accordance with the X-ray structure analysis.
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spelling pubmed-29702222010-12-30 2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine Rivera, Augusto Maldonado, Mauricio Ríos-Motta, Jaime González-Salas, Diego Dacunha-Marinho, Bruno Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title structure, C(18)H(20)N(4), the aromatic rings are almost orthogonal [81.6 (2)°]. The mol­ecule has symmetry 2 since it is situated on a crystallographic twofold axis. There are only weak inter­molecular inter­actions present in the structure, notably C—H⋯π-electron ring inter­actions. The (1)H and (13)C NMR spectra are in accordance with the X-ray structure analysis. International Union of Crystallography 2009-09-26 /pmc/articles/PMC2970222/ /pubmed/21577994 http://dx.doi.org/10.1107/S1600536809038380 Text en © Rivera et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Rivera, Augusto
Maldonado, Mauricio
Ríos-Motta, Jaime
González-Salas, Diego
Dacunha-Marinho, Bruno
2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
title 2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
title_full 2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
title_fullStr 2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
title_full_unstemmed 2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
title_short 2,9-Dimethyl-6H,13H-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
title_sort 2,9-dimethyl-6h,13h-5:12,7:14-dimethano­dibenzo[d,i][1,3,6,8]tetraazecine
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970222/
https://www.ncbi.nlm.nih.gov/pubmed/21577994
http://dx.doi.org/10.1107/S1600536809038380
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