(E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate

In the title compound, C(13)H(9)Cl(2)N(3)O·H(2)O, the 3,4-dichloro­benzene ring is nearly coplanar with the pyridine ring, making a dihedral angle of 4.78 (8)°. Inter­molecular O—H⋯O, O—H⋯N, N—H⋯O and weak C—H⋯O hydrogen bonding is present in the crystal structure.

Detalles Bibliográficos
Autores principales: Bao, Feng-Yu, Zhou, Ying-Xia, Zhang, Hai-Yan, Hui, Su
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970266/
https://www.ncbi.nlm.nih.gov/pubmed/21577807
http://dx.doi.org/10.1107/S1600536809034552
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author Bao, Feng-Yu
Zhou, Ying-Xia
Zhang, Hai-Yan
Hui, Su
author_facet Bao, Feng-Yu
Zhou, Ying-Xia
Zhang, Hai-Yan
Hui, Su
author_sort Bao, Feng-Yu
collection PubMed
description In the title compound, C(13)H(9)Cl(2)N(3)O·H(2)O, the 3,4-dichloro­benzene ring is nearly coplanar with the pyridine ring, making a dihedral angle of 4.78 (8)°. Inter­molecular O—H⋯O, O—H⋯N, N—H⋯O and weak C—H⋯O hydrogen bonding is present in the crystal structure.
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spelling pubmed-29702662010-12-30 (E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate Bao, Feng-Yu Zhou, Ying-Xia Zhang, Hai-Yan Hui, Su Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(13)H(9)Cl(2)N(3)O·H(2)O, the 3,4-dichloro­benzene ring is nearly coplanar with the pyridine ring, making a dihedral angle of 4.78 (8)°. Inter­molecular O—H⋯O, O—H⋯N, N—H⋯O and weak C—H⋯O hydrogen bonding is present in the crystal structure. International Union of Crystallography 2009-09-05 /pmc/articles/PMC2970266/ /pubmed/21577807 http://dx.doi.org/10.1107/S1600536809034552 Text en © Bao et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Bao, Feng-Yu
Zhou, Ying-Xia
Zhang, Hai-Yan
Hui, Su
(E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate
title (E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate
title_full (E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate
title_fullStr (E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate
title_full_unstemmed (E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate
title_short (E)-N′-(3,4-Dichloro­benzyl­idene)nicotino­hydrazide monohydrate
title_sort (e)-n′-(3,4-dichloro­benzyl­idene)nicotino­hydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970266/
https://www.ncbi.nlm.nih.gov/pubmed/21577807
http://dx.doi.org/10.1107/S1600536809034552
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AT huisu en34dichlorobenzylidenenicotinohydrazidemonohydrate

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