(E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate

The title compound, C(14)H(11)N(3)O(3)·CH(4)O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formyl­benzoic acid in methanol. The hydrazone mol­ecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the...

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Detalles Bibliográficos
Autores principales: Li, Wenkuan, Yin, Handong, Wen, Liyuan, Cui, Jichun, Wang, Daqi
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970267/
https://www.ncbi.nlm.nih.gov/pubmed/21578015
http://dx.doi.org/10.1107/S1600536809038902
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author Li, Wenkuan
Yin, Handong
Wen, Liyuan
Cui, Jichun
Wang, Daqi
author_facet Li, Wenkuan
Yin, Handong
Wen, Liyuan
Cui, Jichun
Wang, Daqi
author_sort Li, Wenkuan
collection PubMed
description The title compound, C(14)H(11)N(3)O(3)·CH(4)O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formyl­benzoic acid in methanol. The hydrazone mol­ecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the benzene rings is 12.04 (5)°. In the crystal structure, mol­ecules are linked by O—H⋯N, O—H⋯O and N—H⋯O hydrogen-bonding inter­actions.
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spelling pubmed-29702672010-12-30 (E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate Li, Wenkuan Yin, Handong Wen, Liyuan Cui, Jichun Wang, Daqi Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(14)H(11)N(3)O(3)·CH(4)O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formyl­benzoic acid in methanol. The hydrazone mol­ecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the benzene rings is 12.04 (5)°. In the crystal structure, mol­ecules are linked by O—H⋯N, O—H⋯O and N—H⋯O hydrogen-bonding inter­actions. International Union of Crystallography 2009-09-30 /pmc/articles/PMC2970267/ /pubmed/21578015 http://dx.doi.org/10.1107/S1600536809038902 Text en © Li et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Li, Wenkuan
Yin, Handong
Wen, Liyuan
Cui, Jichun
Wang, Daqi
(E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
title (E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
title_full (E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
title_fullStr (E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
title_full_unstemmed (E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
title_short (E)-2-(Isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
title_sort (e)-2-(isonicotinoylhydrazonometh­yl)benzoic acid methanol monosolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970267/
https://www.ncbi.nlm.nih.gov/pubmed/21578015
http://dx.doi.org/10.1107/S1600536809038902
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AT wenliyuan e2isonicotinoylhydrazonomethylbenzoicacidmethanolmonosolvate
AT cuijichun e2isonicotinoylhydrazonomethylbenzoicacidmethanolmonosolvate
AT wangdaqi e2isonicotinoylhydrazonomethylbenzoicacidmethanolmonosolvate

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