(RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one

In the title compound, C(18)H(18)N(2)O(4), the nitro group, a methyl group, the acetyl group and some atoms of the dihydro­quinolinone group are disordered over two sites with the ratio of occupancies fixed at 0.57:0.43. The relationship between the major and minor components of disorder is that of...

Descripción completa

Detalles Bibliográficos
Autores principales: Wang, Dong’e, Wang, Yu-zhou, Turhong, Muhtar
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970294/
https://www.ncbi.nlm.nih.gov/pubmed/21578001
http://dx.doi.org/10.1107/S160053680903832X
_version_ 1782190404303585280
author Wang, Dong’e
Wang, Yu-zhou
Turhong, Muhtar
author_facet Wang, Dong’e
Wang, Yu-zhou
Turhong, Muhtar
author_sort Wang, Dong’e
collection PubMed
description In the title compound, C(18)H(18)N(2)O(4), the nitro group, a methyl group, the acetyl group and some atoms of the dihydro­quinolinone group are disordered over two sites with the ratio of occupancies fixed at 0.57:0.43. The relationship between the major and minor components of disorder is that of diastereomers. In the crystal structure, inter­molecular N—H⋯O, weak C—H⋯O and C—H⋯π inter­actions link the mol­ecules into two-dimensional layers running parallel to the (010) plane.
format Text
id pubmed-2970294
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29702942010-12-30 (RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one Wang, Dong’e Wang, Yu-zhou Turhong, Muhtar Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(18)H(18)N(2)O(4), the nitro group, a methyl group, the acetyl group and some atoms of the dihydro­quinolinone group are disordered over two sites with the ratio of occupancies fixed at 0.57:0.43. The relationship between the major and minor components of disorder is that of diastereomers. In the crystal structure, inter­molecular N—H⋯O, weak C—H⋯O and C—H⋯π inter­actions link the mol­ecules into two-dimensional layers running parallel to the (010) plane. International Union of Crystallography 2009-09-26 /pmc/articles/PMC2970294/ /pubmed/21578001 http://dx.doi.org/10.1107/S160053680903832X Text en © Wang et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Wang, Dong’e
Wang, Yu-zhou
Turhong, Muhtar
(RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
title (RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
title_full (RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
title_fullStr (RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
title_full_unstemmed (RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
title_short (RS)-3-Acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
title_sort (rs)-3-acetyl-2-methyl-4-(3-nitro­phen­yl)-1,4,5,6,7,8-hexa­hydro­quinolin-5-one
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970294/
https://www.ncbi.nlm.nih.gov/pubmed/21578001
http://dx.doi.org/10.1107/S160053680903832X
work_keys_str_mv AT wangdonge rs3acetyl2methyl43nitrophenyl145678hexahydroquinolin5one
AT wangyuzhou rs3acetyl2methyl43nitrophenyl145678hexahydroquinolin5one
AT turhongmuhtar rs3acetyl2methyl43nitrophenyl145678hexahydroquinolin5one

Ejemplares similares