(E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate

In the title compound, C(14)H(11)N(3)O(3)·H(2)O, the planar [maximum deviation 0.135 (1) Å] 1,3-benzodioxole ring system is oriented at a dihedral angle of 13.93 (7)° with respect to the pyridine ring. Extensive inter­molecular N—H⋯O, O—H⋯O, O—H⋯N and weak C—H⋯O hydrogen bonding is present in the cr...

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Detalles Bibliográficos
Autores principales: Bao, Feng-Yu, Zhang, Hai-Yan, Zhou, Ying-Xia, Hui, Su
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970319/
https://www.ncbi.nlm.nih.gov/pubmed/21577802
http://dx.doi.org/10.1107/S1600536809034503
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author Bao, Feng-Yu
Zhang, Hai-Yan
Zhou, Ying-Xia
Hui, Su
author_facet Bao, Feng-Yu
Zhang, Hai-Yan
Zhou, Ying-Xia
Hui, Su
author_sort Bao, Feng-Yu
collection PubMed
description In the title compound, C(14)H(11)N(3)O(3)·H(2)O, the planar [maximum deviation 0.135 (1) Å] 1,3-benzodioxole ring system is oriented at a dihedral angle of 13.93 (7)° with respect to the pyridine ring. Extensive inter­molecular N—H⋯O, O—H⋯O, O—H⋯N and weak C—H⋯O hydrogen bonding is present in the crystal structure.
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spelling pubmed-29703192010-12-30 (E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate Bao, Feng-Yu Zhang, Hai-Yan Zhou, Ying-Xia Hui, Su Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(11)N(3)O(3)·H(2)O, the planar [maximum deviation 0.135 (1) Å] 1,3-benzodioxole ring system is oriented at a dihedral angle of 13.93 (7)° with respect to the pyridine ring. Extensive inter­molecular N—H⋯O, O—H⋯O, O—H⋯N and weak C—H⋯O hydrogen bonding is present in the crystal structure. International Union of Crystallography 2009-09-05 /pmc/articles/PMC2970319/ /pubmed/21577802 http://dx.doi.org/10.1107/S1600536809034503 Text en © Bao et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Bao, Feng-Yu
Zhang, Hai-Yan
Zhou, Ying-Xia
Hui, Su
(E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
title (E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
title_full (E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
title_fullStr (E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
title_full_unstemmed (E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
title_short (E)-N′-(1,3-Benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
title_sort (e)-n′-(1,3-benzodioxol-5-ylmethyl­ene)nicotinohydrazide monohydrate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970319/
https://www.ncbi.nlm.nih.gov/pubmed/21577802
http://dx.doi.org/10.1107/S1600536809034503
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