6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]

The title compound, C(19)H(21)ClN(6)O(4), is a 1:2 adduct of p-chloro­benzaldehyde and uracil. It crystallizes with two mol­ecules in the asymmetric unit. The two uracil units in the same mol­ecule are connected by a pair of strong N—H⋯O hydrogen bonds. The packing is stabilized by N—H⋯O, C—H⋯O and...

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Detalles Bibliográficos
Autores principales: Das, Subrata, Saikia, Binoy K., Das, Babulal, Saikia, Lakhinath, Thakur, Ashim J.
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970351/
https://www.ncbi.nlm.nih.gov/pubmed/21577875
http://dx.doi.org/10.1107/S1600536809035818
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author Das, Subrata
Saikia, Binoy K.
Das, Babulal
Saikia, Lakhinath
Thakur, Ashim J.
author_facet Das, Subrata
Saikia, Binoy K.
Das, Babulal
Saikia, Lakhinath
Thakur, Ashim J.
author_sort Das, Subrata
collection PubMed
description The title compound, C(19)H(21)ClN(6)O(4), is a 1:2 adduct of p-chloro­benzaldehyde and uracil. It crystallizes with two mol­ecules in the asymmetric unit. The two uracil units in the same mol­ecule are connected by a pair of strong N—H⋯O hydrogen bonds. The packing is stabilized by N—H⋯O, C—H⋯O and C—H⋯N inter­actions.
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spelling pubmed-29703512010-12-30 6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione] Das, Subrata Saikia, Binoy K. Das, Babulal Saikia, Lakhinath Thakur, Ashim J. Acta Crystallogr Sect E Struct Rep Online Organic Papers The title compound, C(19)H(21)ClN(6)O(4), is a 1:2 adduct of p-chloro­benzaldehyde and uracil. It crystallizes with two mol­ecules in the asymmetric unit. The two uracil units in the same mol­ecule are connected by a pair of strong N—H⋯O hydrogen bonds. The packing is stabilized by N—H⋯O, C—H⋯O and C—H⋯N inter­actions. International Union of Crystallography 2009-09-09 /pmc/articles/PMC2970351/ /pubmed/21577875 http://dx.doi.org/10.1107/S1600536809035818 Text en © Das et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Das, Subrata
Saikia, Binoy K.
Das, Babulal
Saikia, Lakhinath
Thakur, Ashim J.
6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]
title 6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]
title_full 6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]
title_fullStr 6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]
title_full_unstemmed 6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]
title_short 6,6′-Diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1H,3H)-dione]
title_sort 6,6′-diamino-1,1′,3,3′-tetra­methyl-5,5′-(4-chloro­benzyl­idene)bis­[pyrimidine-2,4(1h,3h)-dione]
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970351/
https://www.ncbi.nlm.nih.gov/pubmed/21577875
http://dx.doi.org/10.1107/S1600536809035818
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