2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate

The asymmetric unit of the title compound, C(14)H(8)N(2)O(8)·2C(3)H(7)NO or L·2DMF (DMF = N,N-dimethyl­formamide), contains one half of the centrosymmetric mol­ecule L and one solvent mol­ecule, which is disordered between two orientations in a 0.555 (4):0.445 (4) ratio. Inter­molecular O—H⋯O hydrog...

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Detalles Bibliográficos
Autores principales: Ge, Chunhua, Li, Xiangqian, Zhang, Xiangdong, Zhao, Yang, Zhang, Rui
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970400/
https://www.ncbi.nlm.nih.gov/pubmed/21577863
http://dx.doi.org/10.1107/S1600536809035107
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author Ge, Chunhua
Li, Xiangqian
Zhang, Xiangdong
Zhao, Yang
Zhang, Rui
author_facet Ge, Chunhua
Li, Xiangqian
Zhang, Xiangdong
Zhao, Yang
Zhang, Rui
author_sort Ge, Chunhua
collection PubMed
description The asymmetric unit of the title compound, C(14)H(8)N(2)O(8)·2C(3)H(7)NO or L·2DMF (DMF = N,N-dimethyl­formamide), contains one half of the centrosymmetric mol­ecule L and one solvent mol­ecule, which is disordered between two orientations in a 0.555 (4):0.445 (4) ratio. Inter­molecular O—H⋯O hydrogen bonds link one L and two DMF mol­ecules into a centrosymmetric hydrogen-bonded cluster. The crystal packing is further stabilized by weak inter­molecular C—H⋯O hydrogen bonds.
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spelling pubmed-29704002010-12-30 2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate Ge, Chunhua Li, Xiangqian Zhang, Xiangdong Zhao, Yang Zhang, Rui Acta Crystallogr Sect E Struct Rep Online Organic Papers The asymmetric unit of the title compound, C(14)H(8)N(2)O(8)·2C(3)H(7)NO or L·2DMF (DMF = N,N-dimethyl­formamide), contains one half of the centrosymmetric mol­ecule L and one solvent mol­ecule, which is disordered between two orientations in a 0.555 (4):0.445 (4) ratio. Inter­molecular O—H⋯O hydrogen bonds link one L and two DMF mol­ecules into a centrosymmetric hydrogen-bonded cluster. The crystal packing is further stabilized by weak inter­molecular C—H⋯O hydrogen bonds. International Union of Crystallography 2009-09-09 /pmc/articles/PMC2970400/ /pubmed/21577863 http://dx.doi.org/10.1107/S1600536809035107 Text en © Ge et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Ge, Chunhua
Li, Xiangqian
Zhang, Xiangdong
Zhao, Yang
Zhang, Rui
2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate
title 2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate
title_full 2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate
title_fullStr 2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate
title_full_unstemmed 2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate
title_short 2,2′-(1,3,5,7-Tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid N,N-dimethyl­formamide disolvate
title_sort 2,2′-(1,3,5,7-tetra­oxo-1,2,3,5,6,7-hexa­hydro­pyrrolo[3,4-f]isoindole-2,6-di­yl)diacetic acid n,n-dimethyl­formamide disolvate
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970400/
https://www.ncbi.nlm.nih.gov/pubmed/21577863
http://dx.doi.org/10.1107/S1600536809035107
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