(2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph

In the title compound, C(14)H(13)NO(4)S, a sulfonamide derivative of phenyl glycine, the aromatic rings are inclined at a dihedral angle of 28.03 (12)°. In the crystal, O—H⋯O hydrogen bonds link the molecules into chains propagating in [100] and a weak C—H⋯O interaction cross-links the chains in the...

Descripción completa

Detalles Bibliográficos
Autores principales: Khan, Islam Ullah, Sharif, Shahzad, Arshad, Muhammad Nadeem, Ejaz, Idrees, Muhammad
Formato: Texto
Lenguaje:English
Publicado: International Union of Crystallography 2009
Materias:
Organic Papers
Acceso en línea:https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970412/
https://www.ncbi.nlm.nih.gov/pubmed/21577892
http://dx.doi.org/10.1107/S160053680903606X
_version_ 1782190436417273856
author Khan, Islam Ullah
Sharif, Shahzad
Arshad, Muhammad Nadeem
Ejaz,
Idrees, Muhammad
author_facet Khan, Islam Ullah
Sharif, Shahzad
Arshad, Muhammad Nadeem
Ejaz,
Idrees, Muhammad
author_sort Khan, Islam Ullah
collection PubMed
description In the title compound, C(14)H(13)NO(4)S, a sulfonamide derivative of phenyl glycine, the aromatic rings are inclined at a dihedral angle of 28.03 (12)°. In the crystal, O—H⋯O hydrogen bonds link the molecules into chains propagating in [100] and a weak C—H⋯O interaction cross-links the chains in the c-axis direction. In the previously published polymorph, the dihedral angle between the aromatic rings is 45.52 (18)° and the structure is stabilized by three different types of ring motif.
format Text
id pubmed-2970412
institution National Center for Biotechnology Information
language English
publishDate 2009
publisher International Union of Crystallography
record_format MEDLINE/PubMed
spelling pubmed-29704122010-12-30 (2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph Khan, Islam Ullah Sharif, Shahzad Arshad, Muhammad Nadeem Ejaz, Idrees, Muhammad Acta Crystallogr Sect E Struct Rep Online Organic Papers In the title compound, C(14)H(13)NO(4)S, a sulfonamide derivative of phenyl glycine, the aromatic rings are inclined at a dihedral angle of 28.03 (12)°. In the crystal, O—H⋯O hydrogen bonds link the molecules into chains propagating in [100] and a weak C—H⋯O interaction cross-links the chains in the c-axis direction. In the previously published polymorph, the dihedral angle between the aromatic rings is 45.52 (18)° and the structure is stabilized by three different types of ring motif. International Union of Crystallography 2009-09-12 /pmc/articles/PMC2970412/ /pubmed/21577892 http://dx.doi.org/10.1107/S160053680903606X Text en © Khan et al. 2009 http://creativecommons.org/licenses/by/2.0/uk/ This is an open-access article distributed under the terms of the Creative Commons Attribution Licence, which permits unrestricted use, distribution, and reproduction in any medium, provided the original authors and source are cited.
spellingShingle Organic Papers
Khan, Islam Ullah
Sharif, Shahzad
Arshad, Muhammad Nadeem
Ejaz,
Idrees, Muhammad
(2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
title (2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
title_full (2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
title_fullStr (2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
title_full_unstemmed (2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
title_short (2R)-2-Benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
title_sort (2r)-2-benzene­sulfonamido-2-phenyl­ethanoic acid: a new monoclinic polymorph
topic Organic Papers
url https://www.ncbi.nlm.nih.gov/pmc/articles/PMC2970412/
https://www.ncbi.nlm.nih.gov/pubmed/21577892
http://dx.doi.org/10.1107/S160053680903606X
work_keys_str_mv AT khanislamullah 2r2benzenesulfonamido2phenylethanoicacidanewmonoclinicpolymorph
AT sharifshahzad 2r2benzenesulfonamido2phenylethanoicacidanewmonoclinicpolymorph
AT arshadmuhammadnadeem 2r2benzenesulfonamido2phenylethanoicacidanewmonoclinicpolymorph
AT ejaz 2r2benzenesulfonamido2phenylethanoicacidanewmonoclinicpolymorph
AT idreesmuhammad 2r2benzenesulfonamido2phenylethanoicacidanewmonoclinicpolymorph

Ejemplares similares